3,5-Dibromo-4-(phenylmethoxy)benzoic acid

Base Information

Chemical Name:3,5-Dibromo-4-(phenylmethoxy)benzoic acid
CAS No.:501657-81-4
Molecular Formula:C₁₄H₁₀Br₂O₃
Molecular Weight:386.04
Hs Code.:
NSC Number:210571
DSSTox Substance ID:DTXSID501273401

Synonyms:NSC210571;DTXSID501273401;NSC-210571;3,5-Dibromo-4-(phenylmethoxy)benzoic acid;501657-81-4

Suppliers and Price of 3,5-Dibromo-4-(phenylmethoxy)benzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-Dibromo-4-(phenylmethoxy)benzoic acid

Chemical Property:

XLogP3:4.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:385.89762
Heavy Atom Count:19
Complexity:293

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)COC2=C(C=C(C=C2Br)C(=O)O)Br

Technology Process of 3,5-Dibromo-4-(phenylmethoxy)benzoic acid

There total 4 articles about 3,5-Dibromo-4-(phenylmethoxy)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 4-(benzyloxy)-3,5-dibromobenzoic acid methyl ester

: 501657-81-4
3,5-dibromo-4-benzyloxybenzoic acid

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 6h;

Reference yield:

: C₂₁H₁₆Br₂O₃

: 501657-81-4
3,5-dibromo-4-benzyloxybenzoic acid

Guidance literature:: With methanol; lithium hydroxide monohydrate; water; In tetrahydrofuran; for 3h;
DOI:10.1021/jm800435s

Reference yield:

: 3337-62-0
3,5-dibromo-4-hydroxybenzoic acid

: 501657-81-4
3,5-dibromo-4-benzyloxybenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid / 16 h / 80 °C / Cooling with ice

2.1: potassium carbonate / acetone / 0.17 h / 20 °C

2.2: 20 °C

3.1: sodium hydroxide / tetrahydrofuran; water / 6 h / 20 °C

With sulfuric acid; potassium carbonate; sodium hydroxide; In tetrahydrofuran; water; acetone;