1-<2'-deoxy-3',5'-di-O-(p-toluoyl)-α-D-erythro-pentofuranosyl>-2(1H)-pyrimidinone

Base Information

Chemical Name:1-<2'-deoxy-3',5'-di-O-(p-toluoyl)-α-D-erythro-pentofuranosyl>-2(1H)-pyrimidinone
CAS No.:68753-37-7
Molecular Formula:C₂₅H₂₄N₂O₆
Molecular Weight:448.475
Hs Code.:

Synonyms:1-<2'-deoxy-3',5'-di-O-(p-toluoyl)-α-D-erythro-pentofuranosyl>-2(1H)-pyrimidinone

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Chemical Property of 1-<2'-deoxy-3',5'-di-O-(p-toluoyl)-α-D-erythro-pentofuranosyl>-2(1H)-pyrimidinone

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Technology Process of 1-<2'-deoxy-3',5'-di-O-(p-toluoyl)-α-D-erythro-pentofuranosyl>-2(1H)-pyrimidinone

There total 6 articles about 1-<2'-deoxy-3',5'-di-O-(p-toluoyl)-α-D-erythro-pentofuranosyl>-2(1H)-pyrimidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 121012-93-9
2-<2'-deoxy-3',5'-di-O-(p-toluoyl)-β-D-erythro-pentofuranosyloxy>pyrimidine

: 68753-37-7
1-<2'-deoxy-3',5'-di-O-(p-toluoyl)-α-D-erythro-pentofuranosyl>-2(1H)-pyrimidinone

Guidance literature:: With toluene-4-sulfonic acid; In acetonitrile; at 50 ℃; for 12h;

Reference yield: 53.5%

: 4330-21-6
2-deoxy-3,5-di-O-p-toluoyl-α-D-erythro-pentofuranosyl chloride

: 52523-22-5
2-trimethylsilyloxypyrimidine

: 68753-36-6
1-<2'-Desoxy-3',5'-di-O-(p-toluoyl)-β-D-ribofuranosyl>-2(1H)-pyrimidinon

: 68753-37-7
1-<2'-deoxy-3',5'-di-O-(p-toluoyl)-α-D-erythro-pentofuranosyl>-2(1H)-pyrimidinone

Guidance literature:: With tin(IV) chloride; In 1,2-dichloro-ethane; at 35 ℃; for 3h; Solvent;
DOI:10.1016/j.carres.2014.03.018

Reference yield: 31.0%

: 557-01-7
Pyrimidin-2(1H)-one

: 4330-21-6
2-deoxy-3,5-di-O-p-toluoyl-α-D-erythro-pentofuranosyl chloride

: 121012-93-9
2-<2'-deoxy-3',5'-di-O-(p-toluoyl)-β-D-erythro-pentofuranosyloxy>pyrimidine

: 68753-37-7
1-<2'-deoxy-3',5'-di-O-(p-toluoyl)-α-D-erythro-pentofuranosyl>-2(1H)-pyrimidinone

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; for 1h; Product distribution; Ambient temperature; also with other reagents, solvent, times and temp.;