N-benzyloxycarbonyl-N-methyl-2-(4-hydroxy-3-benzyloxyphenyl)-2-acetoxyethylamine 4-O-dibenzylphosphate

Base Information

Chemical Name:N-benzyloxycarbonyl-N-methyl-2-(4-hydroxy-3-benzyloxyphenyl)-2-acetoxyethylamine 4-O-dibenzylphosphate
CAS No.:179616-31-0
Molecular Formula:C₄₀H₄₀NO₉P
Molecular Weight:709.733
Hs Code.:

Synonyms:N-benzyloxycarbonyl-N-methyl-2-(4-hydroxy-3-benzyloxyphenyl)-2-acetoxyethylamine 4-O-dibenzylphosphate

Suppliers and Price of N-benzyloxycarbonyl-N-methyl-2-(4-hydroxy-3-benzyloxyphenyl)-2-acetoxyethylamine 4-O-dibenzylphosphate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-benzyloxycarbonyl-N-methyl-2-(4-hydroxy-3-benzyloxyphenyl)-2-acetoxyethylamine 4-O-dibenzylphosphate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-benzyloxycarbonyl-N-methyl-2-(4-hydroxy-3-benzyloxyphenyl)-2-acetoxyethylamine 4-O-dibenzylphosphate

There total 4 articles about N-benzyloxycarbonyl-N-methyl-2-(4-hydroxy-3-benzyloxyphenyl)-2-acetoxyethylamine 4-O-dibenzylphosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 108-24-7
acetic anhydride

: 179616-30-9
{2-[3-Benzyloxy-4-(bis-benzyloxy-phosphoryloxy)-phenyl]-2-hydroxy-ethyl}-methyl-carbamic acid benzyl ester

: 179616-31-0
N-benzyloxycarbonyl-N-methyl-2-(4-hydroxy-3-benzyloxyphenyl)-2-acetoxyethylamine 4-O-dibenzylphosphate

Guidance literature:: In pyridine; for 4h;
DOI:10.1080/00397919608005221

Reference yield:

: 538-37-4
dibenzyl phosphochloridate

: 179616-31-0
N-benzyloxycarbonyl-N-methyl-2-(4-hydroxy-3-benzyloxyphenyl)-2-acetoxyethylamine 4-O-dibenzylphosphate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) DMF, 2 h, 0-5 deg C, 2.) toluene, 30 min

2: 80 percent / NaBH₄ / methanol / 30 h

3: 96 percent / pyridine / 4 h

With sodium tetrahydroborate; sodium hydride; In pyridine; methanol;
DOI:10.1080/00397919608005221

Reference yield:

: 106148-95-2
3-O-benzyl-N-benzyloxycarbonyladrenalone

: 179616-31-0
N-benzyloxycarbonyl-N-methyl-2-(4-hydroxy-3-benzyloxyphenyl)-2-acetoxyethylamine 4-O-dibenzylphosphate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) DMF, 2 h, 0-5 deg C, 2.) toluene, 30 min

2: 80 percent / NaBH₄ / methanol / 30 h

3: 96 percent / pyridine / 4 h

With sodium tetrahydroborate; sodium hydride; In pyridine; methanol;
DOI:10.1080/00397919608005221