4,4'-[octane-1,8-diylbis(1H-1,2,3-triazol-1,4-diylpropan-3,1-diyloxy)]bis(3-methoxybenzoic acid)

Base Information

Chemical Name:4,4'-[octane-1,8-diylbis(1H-1,2,3-triazol-1,4-diylpropan-3,1-diyloxy)]bis(3-methoxybenzoic acid)
CAS No.:1346263-88-4
Molecular Formula:C₃₄H₄₄N₆O₈
Molecular Weight:664.759
Hs Code.:

Synonyms:4,4'-[octane-1,8-diylbis(1H-1,2,3-triazol-1,4-diylpropan-3,1-diyloxy)]bis(3-methoxybenzoic acid)

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Chemical Property of 4,4'-[octane-1,8-diylbis(1H-1,2,3-triazol-1,4-diylpropan-3,1-diyloxy)]bis(3-methoxybenzoic acid)

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Technology Process of 4,4'-[octane-1,8-diylbis(1H-1,2,3-triazol-1,4-diylpropan-3,1-diyloxy)]bis(3-methoxybenzoic acid)

There total 3 articles about 4,4'-[octane-1,8-diylbis(1H-1,2,3-triazol-1,4-diylpropan-3,1-diyloxy)]bis(3-methoxybenzoic acid) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 98560-17-9
1,8-diazidooctane

: 1346263-87-3
methyl 3-methoxy-4-(pent-4-yn-1-yloxy)benzoate

: 1346263-88-4
4,4'-[octane-1,8-diylbis(1H-1,2,3-triazol-1,4-diylpropan-3,1-diyloxy)]bis(3-methoxybenzoic acid)

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In methanol; dichloromethane; at 20 ℃; for 24h;
DOI:10.1021/jm2009919

Reference yield:

: 14267-92-6
1-chloro-4-pentyne

: 1346263-88-4
4,4'-[octane-1,8-diylbis(1H-1,2,3-triazol-1,4-diylpropan-3,1-diyloxy)]bis(3-methoxybenzoic acid)

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; potassium iodide / acetonitrile / 20 h / Reflux

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / methanol; dichloromethane / 24 h / 20 °C

With copper(ll) sulfate pentahydrate; potassium carbonate; sodium L-ascorbate; potassium iodide; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/jm2009919

Reference yield:

: 3943-74-6
4-hydroxy-3-methoxybenzoic acid methyl ester

: 1346263-88-4
4,4'-[octane-1,8-diylbis(1H-1,2,3-triazol-1,4-diylpropan-3,1-diyloxy)]bis(3-methoxybenzoic acid)

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; potassium iodide / acetonitrile / 20 h / Reflux

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / methanol; dichloromethane / 24 h / 20 °C

With copper(ll) sulfate pentahydrate; potassium carbonate; sodium L-ascorbate; potassium iodide; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/jm2009919