p-tolyl 3-O-benzyl-4-O-p-methoxybenzyl-6-O-tert-butyl-diphenylsilyl-1-thio-α-L-idopyranoside

Base Information

• Chemical Name: p-tolyl 3-O-benzyl-4-O-p-methoxybenzyl-6-O-tert-butyl-diphenylsilyl-1-thio-α-L-idopyranoside
• CAS No.: 1415218-21-1
• Molecular Formula: C₄₄H₅₀O₆SSi
• Molecular Weight: 735.029

Synonyms:p-tolyl 3-O-benzyl-4-O-p-methoxybenzyl-6-O-tert-butyl-diphenylsilyl-1-thio-α-L-idopyranoside

Chemical Property of p-tolyl 3-O-benzyl-4-O-p-methoxybenzyl-6-O-tert-butyl-diphenylsilyl-1-thio-α-L-idopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of p-tolyl 3-O-benzyl-4-O-p-methoxybenzyl-6-O-tert-butyl-diphenylsilyl-1-thio-α-L-idopyranoside

There total 3 articles about p-tolyl 3-O-benzyl-4-O-p-methoxybenzyl-6-O-tert-butyl-diphenylsilyl-1-thio-α-L-idopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

p-tolyl 2-O-benzoyl-3-O-benzyl-4-O-p-methoxybenzyl-6-O-tert-butyl-diphenylsilyl-1-thio-α-L-idopyranoside (1415218-20-0) → p-tolyl 3-O-benzyl-4-O-p-methoxybenzyl-6-O-tert-butyl-diphenylsilyl-1-thio-α-L-idopyranoside (1415218-21-1)

Guidance literature:

p-tolyl 2-O-benzoyl-3-O-benzyl-4-O-p-methoxybenzyl-6-O-tert-butyl-diphenylsilyl-1-thio-α-L-idopyranoside; With sodium methylate; In methanol; dichloromethane; pH=12; Inert atmosphere;

With hydrogenchloride; In methanol; dichloromethane; pH=7; Inert atmosphere;

DOI:10.1002/anie.201205601

Reference yield:

tert-butylchlorodiphenylsilane (58479-61-1) → p-tolyl 3-O-benzyl-4-O-p-methoxybenzyl-6-O-tert-butyl-diphenylsilyl-1-thio-α-L-idopyranoside (1415218-21-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 1H-imidazole / dichloromethane / 20 °C / Inert atmosphere

2.1: sodium methylate / dichloromethane; methanol / pH 12 / Inert atmosphere

2.2: pH 7 / Inert atmosphere

With 1H-imidazole; sodium methylate; In methanol; dichloromethane;

DOI:10.1002/anie.201205601

Reference yield:

C35H36O7S (1242437-69-9) → p-tolyl 3-O-benzyl-4-O-p-methoxybenzyl-6-O-tert-butyl-diphenylsilyl-1-thio-α-L-idopyranoside (1415218-21-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 1H-imidazole / dichloromethane / 20 °C / Inert atmosphere

2.1: sodium methylate / dichloromethane; methanol / pH 12 / Inert atmosphere

2.2: pH 7 / Inert atmosphere

With 1H-imidazole; sodium methylate; In methanol; dichloromethane;

DOI:10.1002/anie.201205601

upstream raw materials:

tert-butylchlorodiphenylsilane

p-tolyl 2-O-benzoyl-3-O-benzyl-4-O-p-methoxybenzyl-6-O-tert-butyl-diphenylsilyl-1-thio-α-L-idopyranoside

C₃₅H₃₆O₇S

Downstream raw materials:

p-tolyl 2-O-levulinoyl-3-O-benzyl-4-O-p-methoxybenzyl-6-O-tert-butyl-diphenylsilyl-1-thio-α-L-idopyranoside

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1415218-21-1 p-tolyl 3-O-benzyl-4-O-p-methoxybenzyl-6-O-tert-butyl-diphenylsilyl-1-thio-α-L-idopyranoside

Send

Send

Metric Ton KG G Pound L ML

Send

Send