Technology Process of C26H18F4N2O4
There total 3 articles about C26H18F4N2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C19H11F4NO4;
With
triethylamine;
In
toluene;
at 100 ℃;
for 1h;
Molecular sieve;
benzyl alcohol;
With
diphenyl phosphoryl azide;
In
toluene;
at 110 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium hydroxide monohydrate; water / methanol / 20 °C
2.1: triethylamine / toluene / 1 h / 100 °C / Molecular sieve
2.2: 110 °C / Inert atmosphere
With
lithium hydroxide monohydrate; water; triethylamine;
In
methanol; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium phosphate; tetrakis(triphenylphosphine) palladium(0) / water; 1,2-dimethoxyethane
2.1: lithium hydroxide monohydrate / methanol; water / 20 °C
3.1: triethylamine / toluene / 1 h / 100 °C / Molecular sieve
3.2: 110 °C / Inert atmosphere
With
potassium phosphate; tetrakis(triphenylphosphine) palladium(0); lithium hydroxide monohydrate; triethylamine;
In
methanol; 1,2-dimethoxyethane; water; toluene;