1-[2-(tert-butyl-dimethyl-silanyloxy)-phenyl]-3-cyclohex-1-enyl-propynone

Base Information

Chemical Name:1-[2-(tert-butyl-dimethyl-silanyloxy)-phenyl]-3-cyclohex-1-enyl-propynone
CAS No.:223511-31-7
Molecular Formula:C₂₁H₂₈O₂Si
Molecular Weight:340.538
Hs Code.:

1-[2-(<i>tert</i>-butyl-dimethyl-silanyloxy)-phenyl]-3-cyclohex-1-enyl-propynone

Synonyms:1-[2-(tert-butyl-dimethyl-silanyloxy)-phenyl]-3-cyclohex-1-enyl-propynone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[2-(tert-butyl-dimethyl-silanyloxy)-phenyl]-3-cyclohex-1-enyl-propynone

Chemical Property:

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Technology Process of 1-[2-(tert-butyl-dimethyl-silanyloxy)-phenyl]-3-cyclohex-1-enyl-propynone

There total 2 articles about 1-[2-(tert-butyl-dimethyl-silanyloxy)-phenyl]-3-cyclohex-1-enyl-propynone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 174362-59-5
C₁₉H₃₄O₃Si₂

: 223511-31-7
1-[2-(tert-butyl-dimethyl-silanyloxy)-phenyl]-3-cyclohex-1-enyl-propynone

Guidance literature:: Multi-step reaction with 2 steps

1: (COCl)2, DMF / CH₂Cl₂ / 0 deg C -> r.t., 18 h

2: CuI, Et₃N / Pd(PPh₃)2Cl₂ / 15 h

With copper(l) iodide; oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; bis-triphenylphosphine-palladium(II) chloride; In dichloromethane;
DOI:10.1016/S0040-4039(99)00279-8

Reference yield:

: 931-49-7
1-ethenylcyclohexene

: 827575-54-2
2-(tert-butyldimethylsilanyloxy)-benzoyl chloride

: 223511-31-7
1-[2-(tert-butyl-dimethyl-silanyloxy)-phenyl]-3-cyclohex-1-enyl-propynone

Guidance literature:: With copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride; for 15h; Yield given;
DOI:10.1016/S0040-4039(99)00279-8