(5-Isopropyl-4-oxo-3-pentafluorophenyl-2-thioxo-imidazolidin-1-yl)-acetaldehyde

Base Information

Chemical Name:(5-Isopropyl-4-oxo-3-pentafluorophenyl-2-thioxo-imidazolidin-1-yl)-acetaldehyde
CAS No.:156522-43-9
Molecular Formula:C₁₄H₁₁F₅N₂O₂S
Molecular Weight:366.312
Hs Code.:

Synonyms:(5-Isopropyl-4-oxo-3-pentafluorophenyl-2-thioxo-imidazolidin-1-yl)-acetaldehyde

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Chemical Property of (5-Isopropyl-4-oxo-3-pentafluorophenyl-2-thioxo-imidazolidin-1-yl)-acetaldehyde

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Technology Process of (5-Isopropyl-4-oxo-3-pentafluorophenyl-2-thioxo-imidazolidin-1-yl)-acetaldehyde

There total 5 articles about (5-Isopropyl-4-oxo-3-pentafluorophenyl-2-thioxo-imidazolidin-1-yl)-acetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: Acetic acid 2-(5-isopropyl-4-oxo-3-pentafluorophenyl-2-thioxo-imidazolidin-1-yl)-1-phenylsulfanyl-ethyl ester

: 156522-43-9
(5-Isopropyl-4-oxo-3-pentafluorophenyl-2-thioxo-imidazolidin-1-yl)-acetaldehyde

Guidance literature:: With sulfuric acid; mercury dichloride; In tetrahydrofuran; water; at 20 - 65 ℃; for 24h;
DOI:10.1016/S0040-4039(00)73094-2

Reference yield:

: 35923-79-6
1,2,3,4,5-pentafluoro-6-isothiocyanatobenzene

: 156522-43-9
(5-Isopropyl-4-oxo-3-pentafluorophenyl-2-thioxo-imidazolidin-1-yl)-acetaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 46 percent / pyridine / 3 h / 45 °C

2: 97 percent / sodium acetate / 5 h / Heating

3: 30 percent / HgCl₂, conc. H₂SO₄ / tetrahydrofuran; H₂O / 24 h / 20 - 65 °C

With sulfuric acid; sodium acetate; mercury dichloride; In tetrahydrofuran; pyridine; water;
DOI:10.1016/S0040-4039(00)73094-2

Reference yield:

: 516-06-3,25609-85-2,7004-03-7,921-10-8
D,L-valine

: 156522-43-9
(5-Isopropyl-4-oxo-3-pentafluorophenyl-2-thioxo-imidazolidin-1-yl)-acetaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: 56 percent / aq. NaOH / 24 h / 10 - 25 °C

2: 46 percent / pyridine / 3 h / 45 °C

3: 97 percent / sodium acetate / 5 h / Heating

4: 30 percent / HgCl₂, conc. H₂SO₄ / tetrahydrofuran; H₂O / 24 h / 20 - 65 °C

With sodium hydroxide; sulfuric acid; sodium acetate; mercury dichloride; In tetrahydrofuran; pyridine; water;
DOI:10.1016/S0040-4039(00)73094-2