C₂₀H₃₁Cl₂NO₃S

Base Information

Chemical Name:C₂₀H₃₁Cl₂NO₃S
CAS No.:1315314-33-0
Molecular Formula:C₂₀H₃₁Cl₂NO₃S
Molecular Weight:436.443
Hs Code.:

C<sub>20</sub>H<sub>31</sub>Cl<sub>2</sub>NO<sub>3</sub>S

Synonyms:C₂₀H₃₁Cl₂NO₃S

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Chemical Property of C₂₀H₃₁Cl₂NO₃S

Chemical Property:

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Technology Process of C₂₀H₃₁Cl₂NO₃S

There total 5 articles about C₂₀H₃₁Cl₂NO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 959051-08-2
5-chloro-pentanoic acid phenyl ester

: 959420-89-4
(+)-(S)-N-[(1E)-5-chloropentylidene]-2-methylpropane-2-sulfinamide

: 1315314-33-0
C₂₀H₃₁Cl₂NO₃S

: 1315314-30-7
(+)-(2R,3S)-7-chloro-2-(3-chloro-propyl)-3-((S)-2-methyl-propane-2-sulfinylamino)-heptanoic acid phenyl ester

Guidance literature:: 5-chloro-pentanoic acid phenyl ester; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

(+)-(S)-N-[(1E)-5-chloropentylidene]-2-methylpropane-2-sulfinamide; In tetrahydrofuran; for 1h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol2015048

Reference yield:

: 14273-86-0
methyl 5-chloropentanoate

: 1315314-33-0
C₂₀H₃₁Cl₂NO₃S

Guidance literature:: Multi-step reaction with 3 steps

1.1: diisobutylaluminium hydride / hexane; dichloromethane / 2.17 h / -60 °C / Inert atmosphere

2.1: copper(II) sulfate / dichloromethane / 18 h / 40 °C / Inert atmosphere

3.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

3.2: 1 h / Inert atmosphere

With diisobutylaluminium hydride; copper(II) sulfate; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ol2015048

Reference yield:

: 20074-80-0
5-chloro-pentanal

: 1315314-33-0
C₂₀H₃₁Cl₂NO₃S

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper(II) sulfate / dichloromethane / 18 h / 40 °C / Inert atmosphere

2.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2.2: 1 h / Inert atmosphere

With copper(II) sulfate; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol2015048