1,1-Dibutoxytrimethylamine

Base Information

• Chemical Name: 1,1-Dibutoxytrimethylamine
• CAS No.: 18503-90-7
• Molecular Formula: C11H25NO2
• Molecular Weight: 203.325
• Hs Code.: 2922199090
• European Community (EC) Number: 242-387-0
• DSSTox Substance ID: DTXSID80171702
• Nikkaji Number: J150.715J
• Wikidata: Q72465270
• Mol file: 18503-90-7.mol

Synonyms:1,1-Dibutoxytrimethylamine;18503-90-7;N,N-Dimethylformamide dibutyl acetal;1,1-dibutoxy-N,N-dimethylmethanamine;N,N-Dimethylformamide di-n-butyl acetal;EINECS 242-387-0;Copper(2+), (tetraethylenepentamine)-, bis(dicyanoaurate(1-));Copper(2+), (tetraethylenepentamine)-, bis[dicyanoaurate(1-)];dimethylformamide dibutylacetal;SCHEMBL134247;C8H23CuN5.2C2AuN2;GSFFXKGTGPMVLM-UHFFFAOYSA-;dimethylformamide di-n-butylacetal;DTXSID80171702;N,N-Dimethylformamidedibutylacetal;Dibutoxy-N,N-dimethylmethanamine #;MFCD00015249;AKOS025311558;N,N-Dimethylformamide di-n-butylacetal;C8-H23-Cu-N5.2C2-Au-N2;Methanamine, 1,1-dibutoxy-N,N-dimethyl-;CS-0449256;D1302;FT-0629538;N,N-DIMETHYLFORMAMIDEDI-N-BUTYLACETAL;W-107787;N,N-Dimethylformamide Dibutyl Acetal [for Esterification];Copper(2), (tetraethylenepentamine)-, bis[dicyanoaurate(1-)];N,N-Dimethylformamide di-n-butyl acetal (for esterification)

Chemical Property of 1,1-Dibutoxytrimethylamine

Chemical Property:

• Appearance/Colour: clear brown
• Vapor Pressure: 0.0589mmHg at 25°C
• Refractive Index: n20/D 1.417
• Boiling Point: 232.5 °C at 760 mmHg
• PKA: 5.22±0.50(Predicted)
• Flash Point: 53 ºC
• PSA: 21.70000
• Density: 0.853
• LogP: 2.46500
• XLogP3: 2.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 9
• Exact Mass: 203.188529040
• Heavy Atom Count: 14
• Complexity: 108

Purity/Quality:

99% ^*data from raw suppliers

1,1-Dibutoxytrimethylamine ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 10-36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: CCCCOC(N(C)C)OCCCC
• Uses: N,N-Dimethylformamide dibutyl acetal is the suitable reagent used for the simultaneous quantification of cocaine and its primary metabolite, benzoyl ecgonine, from a urine matrix by gas-chromatography. It may be used as reagent for the esterification of fatty acids.

Technology Process of 1,1-Dibutoxytrimethylamine

There total 5 articles about 1,1-Dibutoxytrimethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Bis(dimethylamino)acetonitrile (2214-82-6) + sodium butanolate (2372-45-4) → N,N-dimethylformamide di-n-butyl acetal (18503-90-7)

Guidance literature:

In butan-1-ol;

Reference yield:

N,N-dimethylformamide diethyl diacetal (1188-33-6) + butan-1-ol (71-36-3) → N,N-dimethylformamide di-n-butyl acetal (18503-90-7)

Guidance literature:

at 180 ℃;

Reference yield:

N,N-dimethyl-formamide (68-12-2,33513-42-7) + butan-1-ol (71-36-3) → N,N-dimethylformamide di-n-butyl acetal (18503-90-7)

Guidance literature:

Multistep reaction; (i) SOCl₂, (ii) /BRN= 969148/, Na, CHCl₃;

DOI:10.1002/jps.2600600116

upstream raw materials:

Bis(dimethylamino)acetonitrile

sodium butanolate

N,N-dimethyl-formamide dimethyl acetal

butan-1-ol

Downstream raw materials:

Dibutyl carbonate

3-dimethylamino-3-(trifluoromethyl)acrylophenone

butyl (2R,4R)-2-(2-hydroxyphenyl)-3-(S-2,3,4,5,6-pentafluorobenzyl-3-mercaptopropionyl)-4-thiazolidinecarboxylate