8-Methyl-14-phenyl-8,10,12,13,15,16-hexazatetracyclo[7.7.0.02,7.011,15]hexadeca-1(16),2,4,6,9,11,13-heptaene

Base Information

Chemical Name:8-Methyl-14-phenyl-8,10,12,13,15,16-hexazatetracyclo[7.7.0.02,7.011,15]hexadeca-1(16),2,4,6,9,11,13-heptaene
CAS No.:4137-58-0
Molecular Formula:C₁₇H₁₂N₆
Molecular Weight:300.322
Hs Code.:
NSC Number:183513
DSSTox Substance ID:DTXSID60306934
Wikidata:Q82054247

Synonyms:NSC183513;4137-58-0;NSC 183513;DTXSID60306934;NSC-183513

Suppliers and Price of 8-Methyl-14-phenyl-8,10,12,13,15,16-hexazatetracyclo[7.7.0.02,7.011,15]hexadeca-1(16),2,4,6,9,11,13-heptaene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of 8-Methyl-14-phenyl-8,10,12,13,15,16-hexazatetracyclo[7.7.0.02,7.011,15]hexadeca-1(16),2,4,6,9,11,13-heptaene

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:300.11234441
Heavy Atom Count:23
Complexity:439

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN1C2=CC=CC=C2C3=NN4C(=NN=C4N=C31)C5=CC=CC=C5

Technology Process of 8-Methyl-14-phenyl-8,10,12,13,15,16-hexazatetracyclo[7.7.0.02,7.011,15]hexadeca-1(16),2,4,6,9,11,13-heptaene

There total 6 articles about 8-Methyl-14-phenyl-8,10,12,13,15,16-hexazatetracyclo[7.7.0.02,7.011,15]hexadeca-1(16),2,4,6,9,11,13-heptaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 113387-46-5
3-Benzylidenehydrazino-5-methyl-1,2,4-triazino[5,6-b]indole

: 4137-58-0
10-Methyl-3-phenyl-1,2,4-triazolo[4',3':2,3]1,2,4-triazino[5,6-b]indole

Guidance literature:: With sodium hypochlorite; In 1,4-dioxane; water; at 100 ℃; for 0.166667h;
DOI:10.1016/S0014-827X(99)00107-X

Reference yield: 52.0%

: 3-Benzoylhydrazino-5-methyl-1,2,4-triazino[5,6-b]indole

: 4137-58-0
10-Methyl-3-phenyl-1,2,4-triazolo[4',3':2,3]1,2,4-triazino[5,6-b]indole

Guidance literature:: In acetic acid; at 100 ℃; for 3h;
DOI:10.1016/S0014-827X(99)00107-X

Reference yield:

: 3993-27-9
3-hydrazino-5-methyl-1,2,4-triazino[5,6-b]indole

: 4137-58-0
10-Methyl-3-phenyl-1,2,4-triazolo[4',3':2,3]1,2,4-triazino[5,6-b]indole

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / ethanol / 24 h

2: 65 percent / NaOCl / dioxane; H₂O / 0.17 h / 100 °C

With sodium hypochlorite; In 1,4-dioxane; ethanol; water; 1: Condensation / 2: Cyclization;
DOI:10.1016/S0014-827X(99)00107-X