methyl 2-azido-6-O-acetyl-3,4-di-O-benzyl-2-deoxy-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:methyl 2-azido-6-O-acetyl-3,4-di-O-benzyl-2-deoxy-1-thio-β-D-glucopyranoside
CAS No.:1398044-65-9
Molecular Formula:C₂₃H₂₇N₃O₅S
Molecular Weight:457.55
Hs Code.:

Synonyms:methyl 2-azido-6-O-acetyl-3,4-di-O-benzyl-2-deoxy-1-thio-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-azido-6-O-acetyl-3,4-di-O-benzyl-2-deoxy-1-thio-β-D-glucopyranoside

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Technology Process of methyl 2-azido-6-O-acetyl-3,4-di-O-benzyl-2-deoxy-1-thio-β-D-glucopyranoside

There total 6 articles about methyl 2-azido-6-O-acetyl-3,4-di-O-benzyl-2-deoxy-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 501089-59-4
methyl 2-azido-2,3-di-O-benzyl-2-deoxy-thio-β-D-glucopyranoside

: 108-24-7
acetic anhydride

: 1398044-65-9
methyl 2-azido-6-O-acetyl-3,4-di-O-benzyl-2-deoxy-1-thio-β-D-glucopyranoside

Guidance literature:: With pyridine; at 20 ℃; for 6h;
DOI:10.1002/chem.201204519

Reference yield:

: 1398044-64-8
methyl 2-azido-3,4-di-O-benzyl-2-deoxy-1-thio-6-O-trityl-β-D-glucopyranoside

: 64-19-7,77671-22-8
acetic acid

: 1398044-65-9
methyl 2-azido-6-O-acetyl-3,4-di-O-benzyl-2-deoxy-1-thio-β-D-glucopyranoside

Guidance literature:: In water; at 80 ℃; for 8h;

Reference yield:

: C₂₆H₂₇N₃O₄S

: 1398044-65-9
methyl 2-azido-6-O-acetyl-3,4-di-O-benzyl-2-deoxy-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / N,N-dimethyl-formamide / 1 h / 20 °C / Cooling with ice

2: acetic acid / water / 8 h / 80 °C

3: pyridine / 6 h / 20 °C

With pyridine; sodium hydride; acetic acid; In water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201204519