Benzyl 2-[1-(2-pyridinyl)ethylidene]hydrazinecarbodithioate

Base Information

Chemical Name:Benzyl 2-[1-(2-pyridinyl)ethylidene]hydrazinecarbodithioate
CAS No.:26158-47-4
Molecular Formula:C15H15 N3 S2
Molecular Weight:301.436
Hs Code.:2933990090
NSC Number:295641
ChEMBL ID:CHEMBL72739
Mol file:26158-47-4.mol

Synonyms:MLS002701795;Benzyl 2-[1-(2-pyridinyl)ethylidene]hydrazinecarbodithioate;26158-47-4;SMR001565389;NSC295641;CHEMBL72739;SCHEMBL8738870;BDBM80812;cid_3004127;NSC-295641;benzyl N-(1-pyridin-2-ylethylideneamino)carbamodithioate;(phenylmethyl) N-(1-pyridin-2-ylethylideneamino)carbamodithioate;N-[1-(2-pyridyl)ethylideneamino]carbamodithioic acid benzyl ester;N-[1-(2-pyridinyl)ethylideneamino]carbamodithioic acid (phenylmethyl) ester

Suppliers and Price of Benzyl 2-[1-(2-pyridinyl)ethylidene]hydrazinecarbodithioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of Benzyl 2-[1-(2-pyridinyl)ethylidene]hydrazinecarbodithioate

Chemical Property:

Vapor Pressure:1.72E-08mmHg at 25°C
Boiling Point:455.7°Cat760mmHg
Flash Point:229.4°C
PSA：94.67000
Density:1.18g/cm³
LogP:4.00440
XLogP3:3.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:301.07073984
Heavy Atom Count:20
Complexity:338

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=NNC(=S)SCC1=CC=CC=C1)C2=CC=CC=N2
Isomeric SMILES:C/C(=N\NC(=S)SCC1=CC=CC=C1)/C2=CC=CC=N2

Technology Process of Benzyl 2-[1-(2-pyridinyl)ethylidene]hydrazinecarbodithioate

There total 2 articles about Benzyl 2-[1-(2-pyridinyl)ethylidene]hydrazinecarbodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1122-62-9
2-acetylpyridine

: 13331-31-2
S-benzyldithiocarbazate

: 26158-47-4
[1-(2-pyridine)ethylidene]hydrazinecarbodithioic acid phenylmethyl ester

Guidance literature:: In ethanol; for 0.075h; Microwave irradiation;
DOI:10.1080/00958972.2010.489110

Reference yield:

: 26158-47-4
[1-(2-pyridine)ethylidene]hydrazinecarbodithioic acid phenylmethyl ester

Guidance literature:: 2-Acetylpyridin, Benzyldithiocarbazat;

Reference yield: 90.0%

: bis(acetylacetonate)oxidovanadium(IV)

: 26158-47-4
[1-(2-pyridine)ethylidene]hydrazinecarbodithioic acid phenylmethyl ester

: VO(CH₃COCHCOCH₃)(C₅H₄NC(CH₃)NNCSSCH₂C₆H₅)

Guidance literature:: In methanol; byproducts: CH3COCH2COCH3; 1 equiv. of V-compd. was added to dry MeOH soln. of N-base, reflux for 4h, under anaerobic conditions; cooling to ambient temp., solid was filtered off, washed with MeOH, dried in vac., elem. anal.;
DOI:10.1002/1099-0682(200207)2002:7<1749::AID-EJIC1749>3.0.CO;2-G