C₂₂H₂₃N₃O₂

Base Information

Chemical Name:C₂₂H₂₃N₃O₂
CAS No.:1382486-30-7
Molecular Formula:C₂₂H₂₃N₃O₂
Molecular Weight:361.444
Hs Code.:

C<sub>22</sub>H<sub>23</sub>N<sub>3</sub>O<sub>2</sub>

Synonyms:C₂₂H₂₃N₃O₂

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Chemical Property of C₂₂H₂₃N₃O₂

Chemical Property:

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Technology Process of C₂₂H₂₃N₃O₂

There total 4 articles about C₂₂H₂₃N₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1382486-29-4
C₁₆H₁₇N₃O₂

: 110-13-4
2,5-hexanedione

: 1382486-30-7
C₂₂H₂₃N₃O₂

Guidance literature:: With toluene-4-sulfonic acid; In toluene; at 140 ℃; for 5h;

Reference yield:

: 16532-79-9
4-Bromophenylacetonitrile

: 1382486-30-7
C₂₂H₂₃N₃O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 °C

1.2: 0 - 20 °C

2.1: potassium hydroxide / ethanol / 48 h / 110 °C

3.1: thionyl chloride / 0 - 60 °C

4.1: sodium carbonate / tetrahydrofuran / 0.5 h / 120 °C / Microwave irradiation

5.1: toluene-4-sulfonic acid / toluene / 5 h / 140 °C

With thionyl chloride; sodium hydride; sodium carbonate; toluene-4-sulfonic acid; potassium hydroxide; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; toluene; mineral oil;

Reference yield:

: 485828-58-8
1-(4- bromophenyl)cyclobutane-1-carbonitrile

: 1382486-30-7
C₂₂H₂₃N₃O₂

Guidance literature:: Multi-step reaction with 4 steps

1: potassium hydroxide / ethanol / 48 h / 110 °C

2: thionyl chloride / 0 - 60 °C

3: sodium carbonate / tetrahydrofuran / 0.5 h / 120 °C / Microwave irradiation

4: toluene-4-sulfonic acid / toluene / 5 h / 140 °C

With thionyl chloride; sodium carbonate; toluene-4-sulfonic acid; potassium hydroxide; In tetrahydrofuran; ethanol; toluene;