N-[(R)-3-dodecanoyloxytetradecanoyl] O-bis(phenyloxy)phosphoryl DL-homoserine benzyl ester

Base Information

Chemical Name:N-[(R)-3-dodecanoyloxytetradecanoyl] O-bis(phenyloxy)phosphoryl DL-homoserine benzyl ester
CAS No.:253586-92-4
Molecular Formula:C₄₉H₇₂NO₉P
Molecular Weight:850.086
Hs Code.:

Synonyms:N-[(R)-3-dodecanoyloxytetradecanoyl] O-bis(phenyloxy)phosphoryl DL-homoserine benzyl ester

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Chemical Property of N-[(R)-3-dodecanoyloxytetradecanoyl] O-bis(phenyloxy)phosphoryl DL-homoserine benzyl ester

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Technology Process of N-[(R)-3-dodecanoyloxytetradecanoyl] O-bis(phenyloxy)phosphoryl DL-homoserine benzyl ester

There total 7 articles about N-[(R)-3-dodecanoyloxytetradecanoyl] O-bis(phenyloxy)phosphoryl DL-homoserine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.1%

: 38308-96-2
benzyl O-(diphenyloxyphosphoryl)-DL-homoserinate

: 253586-92-4
N-[(R)-3-dodecanoyloxytetradecanoyl] O-bis(phenyloxy)phosphoryl DL-homoserine benzyl ester

Guidance literature:: (3R)-3-dodecanoyloxytetradecanoic acid; With 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; at -15 ℃; for 0.5h;

benzyl O-(diphenyloxyphosphoryl)-DL-homoserinate; With triethylamine; In tetrahydrofuran; at 20 ℃;

Reference yield: 87.0%

: O-bis(phenyloxy)phosphoryl DL-homoserine benzyl ester trifluoroacetate

: 107856-74-6
C₂₆H₅₀O₄

: 253586-92-4
N-[(R)-3-dodecanoyloxytetradecanoyl] O-bis(phenyloxy)phosphoryl DL-homoserine benzyl ester

Guidance literature:: C₂₆H₅₀O₄; With 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; at -15 ℃; for 0.5h;

O-bis(phenyloxy)phosphoryl DL-homoserine benzyl ester trifluoroacetate; With triethylamine; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/jm060482a

Reference yield:

: 914499-86-8
benzyl (R)-3-dodecanoyloxytetradecanoate

: 253586-92-4
N-[(R)-3-dodecanoyloxytetradecanoyl] O-bis(phenyloxy)phosphoryl DL-homoserine benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 86 percent / H₂ / Pd/C / ethyl acetate; ethanol / 3 h / 20 °C / atmospheric pressure

2.1: N-methylmorpholine; isobutyl chloroformate / tetrahydrofuran / 0.5 h / -15 °C

2.2: 87 percent / Et₃N / tetrahydrofuran / 20 °C

With 4-methyl-morpholine; hydrogen; isobutyl chloroformate; palladium on activated charcoal; In tetrahydrofuran; ethanol; ethyl acetate;
DOI:10.1021/jm060482a