butyl 4-(4-methoxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate

Base Information

Chemical Name:butyl 4-(4-methoxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate
CAS No.:1600526-53-1
Molecular Formula:C₂₈H₄₇NO₅
Molecular Weight:477.685
Hs Code.:

Synonyms:butyl 4-(4-methoxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate

Suppliers and Price of butyl 4-(4-methoxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of butyl 4-(4-methoxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of butyl 4-(4-methoxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate

There total 6 articles about butyl 4-(4-methoxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1600526-52-0
butyl 4-(4-hydroxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate

: 77-78-1
dimethyl sulfate

: 1600526-53-1
butyl 4-(4-methoxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate

Guidance literature:: With potassium carbonate; In acetone; Reflux;

Reference yield:

: 4460-86-0,14374-62-0
asaraldehyde

: 1600526-53-1
butyl 4-(4-methoxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate

Guidance literature:: Multi-step reaction with 6 steps

1.1: dihydrogen peroxide; sulfuric acid / methanol / 2 h / 20 °C / Inert atmosphere; Reflux

2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 - 20 °C / Inert atmosphere

2.2: 13 h / 20 °C

3.1: N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium / tetrahydrofuran; hexane / 2.08 h / -40 - 0 °C

3.2: 15 h / 0 - 20 °C / Inert atmosphere

4.1: ammonium cerium (IV) nitrate; water / acetonitrile / 3.5 h / -7 - 20 °C

5.1: potassium tert-butylate / dichloromethane / 20 h / 20 °C / Inert atmosphere

6.1: potassium carbonate / acetone / Reflux

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; ammonium cerium (IV) nitrate; sulfuric acid; potassium tert-butylate; water; dihydrogen peroxide; sodium hydride; potassium carbonate; In tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl-formamide; acetone; acetonitrile;

Reference yield:

: 20491-91-2
2,4,5-trimethoxyphenol

: 1600526-53-1
butyl 4-(4-methoxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 - 20 °C / Inert atmosphere

1.2: 13 h / 20 °C

2.1: N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium / tetrahydrofuran; hexane / 2.08 h / -40 - 0 °C

2.2: 15 h / 0 - 20 °C / Inert atmosphere

3.1: ammonium cerium (IV) nitrate; water / acetonitrile / 3.5 h / -7 - 20 °C

4.1: potassium tert-butylate / dichloromethane / 20 h / 20 °C / Inert atmosphere

5.1: potassium carbonate / acetone / Reflux

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; ammonium cerium (IV) nitrate; potassium tert-butylate; water; sodium hydride; potassium carbonate; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; acetone; acetonitrile;