3,6-bis(acetoxymethyl)catechol diacetate

Base Information

• Chemical Name: 3,6-bis(acetoxymethyl)catechol diacetate
• CAS No.: 6452-94-4
• Molecular Formula: C₁₆H₁₈O₈
• Molecular Weight: 338.314
• Mol file: 6452-94-4.mol

Synonyms:3,6-bis(acetoxymethyl)catechol diacetate

Chemical Property of 3,6-bis(acetoxymethyl)catechol diacetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,6-bis(acetoxymethyl)catechol diacetate

There total 5 articles about 3,6-bis(acetoxymethyl)catechol diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzene-1,2-diol (120-80-9,19481-10-8,37349-32-9) → 3,6-bis(acetoxymethyl)catechol diacetate (6452-94-4)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol; benzene / 0.5 h / Heating

2: (i) HCO₂H, (ii) /BRN= 385737/, NaOAc

In ethanol; benzene;

DOI:10.1021/jo01032a040

Reference yield:

benzene-1,2-diol (120-80-9,19481-10-8,37349-32-9) → 3,6-bis(acetoxymethyl)catechol diacetate (6452-94-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / ethanol / 96 h / 25 °C

2: 18 h / Heating

In ethanol;

Reference yield:

3,6-bis-morpholin-4-ylmethyl-benzene-1,2-diol (25163-62-6) + acetic anhydride (108-24-7) → 3,6-bis(acetoxymethyl)catechol diacetate (6452-94-4)

Guidance literature:

Heating;

DOI:10.1021/jo01032a040

upstream raw materials:

3,8-dimethyl-2,3,4,7,8,9-hexahydro-benzo[1,2-e;4,3-e']bis[1,3]oxazine

acetic anhydride

3,6-bis-morpholin-4-ylmethyl-benzene-1,2-diol

benzene-1,2-diol

Downstream raw materials:

3,6-Dimethylcatechol

Acetic acid 2-acetoxy-3,6-dimethyl-phenyl ester

3,6-Bis-brommethyl-2-acetoxyphenol

2,3-diacetoxy-1,4-bis-bromomethyl-benzene

Refernces