oxovanadium(V)trimesityl

Base Information

Chemical Name:oxovanadium(V)trimesityl
CAS No.:82364-94-1
Molecular Formula:C₂₇H₃₃OV
Molecular Weight:424.5
Hs Code.:

Synonyms:oxovanadium(V)trimesityl

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Chemical Property of oxovanadium(V)trimesityl

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Technology Process of oxovanadium(V)trimesityl

There total 3 articles about oxovanadium(V)trimesityl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 79738-18-4
[V(mesityl)3(THF)]

: 82364-94-1
oxovanadium(V)trimesityl

Guidance literature:: With styrene oxide or OCH₂CHCH₂CH₃; In tetrahydrofuran; N2; soln. stirred for 30 min; concn. to drynesss, extn. with n-hexane, soln. obtained was filtered, concd., elem. anal.;

Reference yield: 83.0%

: 96-09-3
styrene oxide

: 79738-18-4
[V(mesityl)3(THF)]

: 82364-94-1
oxovanadium(V)trimesityl

Guidance literature:: In tetrahydrofuran; byproducts: styrene; oxidn. of the vanadium complex in THF with styrene oxide at room temp.; crystn. (n-hexane);
DOI:10.1039/c39910000762

Reference yield: 66.0%

: Li⁽¹⁺⁾*VO(C₆H₂(CH₃)3)3^(1-)*3.25C₄H₈O = LiVO(C₆H₂(CH₃)3)3(C₄H₈O)3.25

: 82364-94-1
oxovanadium(V)trimesityl

Guidance literature:: With C₆Cl₄O₂; In diethyl ether; byproducts: C6Cl4O2Li; (inert), V-complex stirred in the darkness with C6Cl4O2 in ether for at least 8 h at room temp.; left to stand overnight, filtered, cooled, pptn. removed, dried in vacuo, elem. anal.;