C₄₁H₅₃IO₅

Base Information

Chemical Name:C₄₁H₅₃IO₅
CAS No.:1266102-67-3
Molecular Formula:C₄₁H₅₃IO₅
Molecular Weight:752.773
Hs Code.:

C<sub>41</sub>H<sub>53</sub>IO<sub>5</sub>

Synonyms:C₄₁H₅₃IO₅

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Chemical Property of C₄₁H₅₃IO₅

Chemical Property:

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Technology Process of C₄₁H₅₃IO₅

There total 12 articles about C₄₁H₅₃IO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1266102-44-6
C₄₁H₅₄O₆

: 1266102-67-3
C₄₁H₅₃IO₅

Guidance literature:: With 1H-imidazole; iodine; triphenylphosphine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jo102054r

Reference yield:

: 1246949-44-9
3-OTBS-11-ketotigogenin

: 1266102-67-3
C₄₁H₅₃IO₅

Guidance literature:: Multi-step reaction with 6 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3: lithium aluminium tetrahydride / tetrahydrofuran / -10 °C / Inert atmosphere; Reflux

4: pyridine; dmap / 6 h / Inert atmosphere; Reflux

5: sodium cyanoborohydride; acetic acid / 1.5 h / 20 °C / Inert atmosphere

6: 1H-imidazole; iodine; triphenylphosphine / dichloromethane / 0 - 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; dmap; lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; iodine; sodium cyanoborohydride; acetic acid; triphenylphosphine; In tetrahydrofuran; dichloromethane; 2: Mitsunobu reaction;
DOI:10.1021/jo102054r

Reference yield:

: 1246949-45-0
C₃₄H₄₆O₅

: 1266102-67-3
C₄₁H₅₃IO₅

Guidance literature:: Multi-step reaction with 4 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / -10 °C / Inert atmosphere; Reflux

2: pyridine; dmap / 6 h / Inert atmosphere; Reflux

3: sodium cyanoborohydride; acetic acid / 1.5 h / 20 °C / Inert atmosphere

4: 1H-imidazole; iodine; triphenylphosphine / dichloromethane / 0 - 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; dmap; lithium aluminium tetrahydride; iodine; sodium cyanoborohydride; acetic acid; triphenylphosphine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo102054r