1,1,2,3-tetrakis(2,4,6-triisopropylphenyl)trisilacyclopropene

Base Information

• Chemical Name: 1,1,2,3-tetrakis(2,4,6-triisopropylphenyl)trisilacyclopropene
• CAS No.: 1393369-86-2
• Molecular Formula: C₆₀H₉₂Si₃
• Molecular Weight: 897.647
• Mol file: 1393369-86-2.mol

Synonyms:1,1,2,3-tetrakis(2,4,6-triisopropylphenyl)trisilacyclopropene

Chemical Property of 1,1,2,3-tetrakis(2,4,6-triisopropylphenyl)trisilacyclopropene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,1,2,3-tetrakis(2,4,6-triisopropylphenyl)trisilacyclopropene

There total 4 articles about 1,1,2,3-tetrakis(2,4,6-triisopropylphenyl)trisilacyclopropene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

Tip2Si=Si(Tip)Si(Tip)Cl2 → 1,1,2,3-tetrakis(2,4,6-triisopropylphenyl)trisilacyclopropene (1393369-86-2)

Guidance literature:

With magnesium; In diethyl ether; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1002/anie.201202277

Reference yield:

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) → 1,1,2,3-tetrakis(2,4,6-triisopropylphenyl)trisilacyclopropene (1393369-86-2)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene / 25 °C / Inert atmosphere

2: 170 °C / Inert atmosphere

In benzene;

DOI:10.1002/anie.201711833

Reference yield:

2-phenyl-1-(2,4,6-triisopropylphenyl)-1-(1,2,2-tris(2,4,6-triisopropylphenyl)disilenyl)silirane → 1,1,2,3-tetrakis(2,4,6-triisopropylphenyl)trisilacyclopropene (1393369-86-2)

Guidance literature:

at 170 ℃; Inert atmosphere;

DOI:10.1002/anie.201711833

upstream raw materials:

styrene