Technology Process of C14H16O
There total 4 articles about C14H16O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
Hoveyda-Grubbs catalyst second generation;
In
dichloromethane;
at 20 ℃;
for 1h;
Inert atmosphere;
DOI:10.1021/ol102982b
- Guidance literature:
-
Multi-step reaction with 2 steps
1: bis(1,5-cyclooctadiene)nickel (0); triphenylphosphine / toluene / 14 h / 20 °C / Inert atmosphere
2: Hoveyda-Grubbs catalyst second generation / dichloromethane / 1 h / 20 °C / Inert atmosphere
With
bis(1,5-cyclooctadiene)nickel (0); Hoveyda-Grubbs catalyst second generation; triphenylphosphine;
In
dichloromethane; toluene;
DOI:10.1021/ol102982b
- Guidance literature:
-
Multi-step reaction with 4 steps
1: chromium dichloride / tetrahydrofuran / 0 °C / Inert atmosphere
2: bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 4 h / 40 °C / 2585.81 Torr / Inert atmosphere
3: bis(1,5-cyclooctadiene)nickel (0); triphenylphosphine / toluene / 14 h / 20 °C / Inert atmosphere
4: Hoveyda-Grubbs catalyst second generation / dichloromethane / 1 h / 20 °C / Inert atmosphere
With
chromium dichloride; bis-triphenylphosphine-palladium(II) chloride; bis(1,5-cyclooctadiene)nickel (0); Hoveyda-Grubbs catalyst second generation; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; toluene;
2: carbonylative Stille coupling;
DOI:10.1021/ol102982b