(1R,2S)-2-(p-dimethylaminobenzoyl)aminocycloheptanol

Base Information

• Chemical Name: (1R,2S)-2-(p-dimethylaminobenzoyl)aminocycloheptanol
• CAS No.: 415693-38-8
• Molecular Formula: C₁₆H₂₄N₂O₂
• Molecular Weight: 276.379

Synonyms:(1R,2S)-2-(p-dimethylaminobenzoyl)aminocycloheptanol

Chemical Property of (1R,2S)-2-(p-dimethylaminobenzoyl)aminocycloheptanol

Chemical Property:

Purity/Quality:

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Technology Process of (1R,2S)-2-(p-dimethylaminobenzoyl)aminocycloheptanol

There total 2 articles about (1R,2S)-2-(p-dimethylaminobenzoyl)aminocycloheptanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dl-cis-2-(p-dimethylaminobenzoyl)aminocycloheptanol → (1R,2S)-2-(p-dimethylaminobenzoyl)aminocycloheptanol (415693-38-8)

Guidance literature:

With 2,3,5-trimethyl-pyridine; 6-(2-C₁₀H₇-CH₂)-1-(py-4-yl)octahydrocyclopenta[b]pyrrol-6-ol; 2-Methylpropionic anhydride; In dichloromethane; at 20 ℃; for 9h;

DOI:10.1039/b108753c

Reference yield:

cis-2-aminocycloheptanol (932-57-0,42565-73-1,89854-90-0,145166-04-7) → (1R,2S)-2-(p-dimethylaminobenzoyl)aminocycloheptanol (415693-38-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 67 percent / triethylamine; 4-dimethylaminopyridine / CH₂Cl₂ / 43 h / 20 °C

2: (i-PrCO)2O; collidine; 6-(2-C₁₀H₇-CH₂)-1-(py-4-yl)octahydrocyclopenta[b]pyrrol-6-ol / CH₂Cl₂ / 9 h / 20 °C

With 2,3,5-trimethyl-pyridine; dmap; 6-(2-C₁₀H₇-CH₂)-1-(py-4-yl)octahydrocyclopenta[b]pyrrol-6-ol; 2-Methylpropionic anhydride; triethylamine; In dichloromethane;

DOI:10.1039/b108753c

upstream raw materials:

cis-2-aminocycloheptanol

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