C₅₃H₅₇N₂O₂⁽¹⁺⁾*Br^(1-)

Base Information

• Chemical Name: C₅₃H₅₇N₂O₂⁽¹⁺⁾*Br^(1-)
• CAS No.: 1606161-15-2
• Molecular Formula: Br*C₅₃H₅₇N₂O₂
• Molecular Weight: 833.952
• Mol file: 1606161-15-2.mol

Synonyms:C₅₃H₅₇N₂O₂⁽¹⁺⁾*Br^(1-)

Chemical Property of C₅₃H₅₇N₂O₂⁽¹⁺⁾*Br^(1-)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₃H₅₇N₂O₂⁽¹⁺⁾*Br^(1-)

There total 4 articles about C₅₃H₅₇N₂O₂⁽¹⁺⁾*Br^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

1H-imidazole (288-32-4) + 2-(bromomethyl)-4,6-bis(α,α-dimethylbenzyl)phenol (1352040-68-6) → C53H57N2O2(1+)*Br(1-) (1606161-15-2)

Guidance literature:

With sodium hydrogencarbonate; In tetrahydrofuran; for 12h; Inert atmosphere; Schlenk technique; Reflux;

DOI:10.1016/j.jorganchem.2013.11.041

Reference yield:

2,4-di-cumylphenol (2772-45-4,106060-52-0) → C53H57N2O2(1+)*Br(1-) (1606161-15-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: acetic acid / 2 h / 20 °C

1.2: 0.5 h / 20 °C

2.1: sodium hydrogencarbonate / tetrahydrofuran / 12 h / Inert atmosphere; Schlenk technique; Reflux

With sodium hydrogencarbonate; acetic acid; In tetrahydrofuran;

DOI:10.1016/j.jorganchem.2013.11.041

Reference yield:

2,4-di-cumylphenol (2772-45-4,106060-52-0) → C28H30N2O (1606161-16-3) + C53H57N2O2(1+)*Br(1-) (1606161-15-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: acetic acid / 2 h / 20 °C

1.2: 0.5 h / 20 °C

2.1: sodium hydrogencarbonate / tetrahydrofuran / Heating

With sodium hydrogencarbonate; acetic acid; In tetrahydrofuran;

DOI:10.1016/j.jorganchem.2013.11.041

upstream raw materials:

1H-imidazole

2-(bromomethyl)-4,6-bis(α,α-dimethylbenzyl)phenol

2,4-di-cumylphenol