C₃₄H₄₂O₅SSi

Base Information

Chemical Name:C₃₄H₄₂O₅SSi
CAS No.:113132-98-2
Molecular Formula:C₃₄H₄₂O₅SSi
Molecular Weight:590.856
Hs Code.:

C<sub>34</sub>H<sub>42</sub>O<sub>5</sub>SSi

Synonyms:C₃₄H₄₂O₅SSi

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Chemical Property of C₃₄H₄₂O₅SSi

Chemical Property:

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Technology Process of C₃₄H₄₂O₅SSi

There total 8 articles about C₃₄H₄₂O₅SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78725-65-2
3-(2,3-dimethoxyphenyl)-1-propyn-3-ol

: 113132-98-2
C₃₄H₄₂O₅SSi

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / Jones reagent / CH₂Cl₂; diethyl ether / 0.5 h / 0 °C

2: 2.) 2,3-dichloro-5,6-dicyano-1,4-benzoquinone (DDQ) / 1.) toluene, 134 deg C, 72 h, 2.) dioxane, 70 deg C, 15.5 h

With jones reagent; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In diethyl ether; dichloromethane;
DOI:10.1021/jo00243a001

Reference yield:

: 113132-91-5
4-cyano-1-(trimethylsiloxy)-3-(trimethylsilyl)-1,4-cyclohexadiene

: 113132-98-2
C₃₄H₄₂O₅SSi

Guidance literature:: Multi-step reaction with 6 steps

1: 88 percent / camphorsulfonic acid / tetrahydrofuran / 216 h / Ambient temperature

2: 86 percent / i-Bu₂AlH (Dibal) / CH₂Cl₂; hexane / 5 h / -78 °C

3: 1.) NaH / 1.) THF, 30 min, 2.) THF, RT, 5.5 h

4: 99 percent / i-Bu₂AlH (Dibal) / CH₂Cl₂; hexane / 1.5 h / -78 °C

5: 89 percent / n-Bu₃P / tetrahydrofuran / 1 h / Ambient temperature

6: 2.) 2,3-dichloro-5,6-dicyano-1,4-benzoquinone (DDQ) / 1.) toluene, 134 deg C, 72 h, 2.) dioxane, 70 deg C, 15.5 h

With tributylphosphine; camphor-10-sulfonic acid; sodium hydride; diisobutylaluminium hydride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/jo00243a001

Reference yield:

: 113132-92-6
3,3-Dimethyl-10-trimethylsilanyl-1,5-dioxa-spiro[5.5]undec-8-ene-9-carbonitrile

: 113132-98-2
C₃₄H₄₂O₅SSi

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / i-Bu₂AlH (Dibal) / CH₂Cl₂; hexane / 5 h / -78 °C

2: 1.) NaH / 1.) THF, 30 min, 2.) THF, RT, 5.5 h

3: 99 percent / i-Bu₂AlH (Dibal) / CH₂Cl₂; hexane / 1.5 h / -78 °C

4: 89 percent / n-Bu₃P / tetrahydrofuran / 1 h / Ambient temperature

5: 2.) 2,3-dichloro-5,6-dicyano-1,4-benzoquinone (DDQ) / 1.) toluene, 134 deg C, 72 h, 2.) dioxane, 70 deg C, 15.5 h

With tributylphosphine; sodium hydride; diisobutylaluminium hydride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/jo00243a001