tert-butyl 4--N-ethylamino>benzoate

Base Information

Chemical Name:tert-butyl 4--N-ethylamino>benzoate
CAS No.:161879-11-4
Molecular Formula:C₂₃H₂₇N₃O₃
Molecular Weight:393.486
Hs Code.:

tert-butyl 4-<N-<(3,4-dihydro-2-methyl-4-oxo-6-quinazolinyl)methyl>-N-ethylamino>benzoate

Synonyms:tert-butyl 4--N-ethylamino>benzoate

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Chemical Property of tert-butyl 4--N-ethylamino>benzoate

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Technology Process of tert-butyl 4--N-ethylamino>benzoate

There total 1 articles about tert-butyl 4--N-ethylamino>benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 112888-43-4
4(3H)-oxo-6-(bromomethyl)-2-methyl quinazoline

: tert-butyl 4-(ethylamino)benzoate

: 161879-11-4
tert-butyl 4--N-ethylamino>benzoate

Guidance literature:: With calcium carbonate; In N,N-dimethyl acetamide; at 50 ℃; for 20h;
DOI:10.1021/jm00046a014

Reference yield: 97.0%

: 161879-11-4
tert-butyl 4--N-ethylamino>benzoate

: 76-05-1
trifluoroacetic acid

: 4--N-ethylamino>benzoic acid trifluoroacetate salt

Guidance literature:: for 0.333333h;
DOI:10.1021/jm00046a014

Reference yield:

: 161879-11-4
tert-butyl 4--N-ethylamino>benzoate

: (S)-4-((S)-1-Carboxy-ethylcarbamoyl)-2-{4-[ethyl-(2-methyl-4-oxo-3,4-dihydro-quinazolin-6-ylmethyl)-amino]-benzoylamino}-butyric acid; compound with trifluoro-acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / 0.33 h

2: 74 percent / diethyl cyanophosphoridate, Et₃N / dimethylformamide / 2 h / Ambient temperature

3: 81 percent / 1 h / Ambient temperature

With diethyl cyanophosphoridate; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1021/jm00046a014