((2E,6E)-9-(3-bromophenyl)-2,6-dimethyl-9-(phenylsulfonyl)nona-2,6-dienyloxy)(tert-butyl)diphenylsilane

Base Information

Chemical Name:((2E,6E)-9-(3-bromophenyl)-2,6-dimethyl-9-(phenylsulfonyl)nona-2,6-dienyloxy)(tert-butyl)diphenylsilane
CAS No.:947588-46-7
Molecular Formula:C₃₉H₄₅BrO₃SSi
Molecular Weight:701.84
Hs Code.:

Synonyms:((2E,6E)-9-(3-bromophenyl)-2,6-dimethyl-9-(phenylsulfonyl)nona-2,6-dienyloxy)(tert-butyl)diphenylsilane

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Chemical Property of ((2E,6E)-9-(3-bromophenyl)-2,6-dimethyl-9-(phenylsulfonyl)nona-2,6-dienyloxy)(tert-butyl)diphenylsilane

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Technology Process of ((2E,6E)-9-(3-bromophenyl)-2,6-dimethyl-9-(phenylsulfonyl)nona-2,6-dienyloxy)(tert-butyl)diphenylsilane

There total 2 articles about ((2E,6E)-9-(3-bromophenyl)-2,6-dimethyl-9-(phenylsulfonyl)nona-2,6-dienyloxy)(tert-butyl)diphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 881075-33-8
(2E,6E)-8-(tert-butyldiphenylsilyloxy)geranyl bromide

: 130891-01-9
1-bromo-3-((phenylsulfonyl)methyl)benzene

: 947588-46-7
((2E,6E)-9-(3-bromophenyl)-2,6-dimethyl-9-(phenylsulfonyl)nona-2,6-dienyloxy)(tert-butyl)diphenylsilane

Guidance literature:: 1-bromo-3-((phenylsulfonyl)methyl)benzene; With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.333333h;

(2E,6E)-8-(tert-butyldiphenylsilyloxy)geranyl bromide; In tetrahydrofuran; hexane; at -78 ℃; for 12h;

With water; ammonium chloride; In tetrahydrofuran; hexane;

Reference yield:

: 1028386-60-8
(6E)-8-(tert-butyldiphenylsilyloxy)geranyl chloride

: 130891-01-9
1-bromo-3-((phenylsulfonyl)methyl)benzene

: 947588-46-7
((2E,6E)-9-(3-bromophenyl)-2,6-dimethyl-9-(phenylsulfonyl)nona-2,6-dienyloxy)(tert-butyl)diphenylsilane

Guidance literature:: 1-bromo-3-((phenylsulfonyl)methyl)benzene; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃;

(6E)-8-(tert-butyldiphenylsilyloxy)geranyl chloride; In tetrahydrofuran; at -78 ℃; for 12h;

With water; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/ol800499p