N-p.dimethylaminophenyl hydroxymethyl-2 methyl-5 diphenyl-3,4 pyrrole

Base Information

• Chemical Name: N-p.dimethylaminophenyl hydroxymethyl-2 methyl-5 diphenyl-3,4 pyrrole
• CAS No.: 106919-97-5
• Molecular Formula: C₂₆H₂₆N₂O
• Molecular Weight: 382.505

Synonyms:N-p.dimethylaminophenyl hydroxymethyl-2 methyl-5 diphenyl-3,4 pyrrole

Chemical Property of N-p.dimethylaminophenyl hydroxymethyl-2 methyl-5 diphenyl-3,4 pyrrole

Chemical Property:

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Technology Process of N-p.dimethylaminophenyl hydroxymethyl-2 methyl-5 diphenyl-3,4 pyrrole

There total 4 articles about N-p.dimethylaminophenyl hydroxymethyl-2 methyl-5 diphenyl-3,4 pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

N-p.dimethylaminophenyl methyl-5 diphenyl-3,4 pyrrolecarbaldehyde-2 (106920-00-7) → N-p.dimethylaminophenyl hydroxymethyl-2 methyl-5 diphenyl-3,4 pyrrole (106919-97-5)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; for 1h; Ambient temperature;

DOI:10.1016/S0040-4020(01)87354-3

Reference yield: 13.0%

N-p.dimethylaminophenyl methyl-5 diphenyl-3,4 pyrrolecarbaldehyde-2 (106920-00-7) → N-p.dimethylaminophenyl dimethyl-2,5 diphenyl-3,4 pyrrole (106920-02-9) + N-p.dimethylaminophenyl hydroxymethyl-2 methyl-5 diphenyl-3,4 pyrrole (106919-97-5)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; for 33h; Heating;

DOI:10.1016/S0040-4020(01)87354-3

Reference yield: 10.0%

2,5-dimethyl-3,4-diphenylcyclopenta-2,4-dione dimer (13360-84-4,38883-84-0) + p-dimethylaminonitrosobenzene (138-89-6) → N-p.dimethylaminophenyl hydroxymethyl-2 methyl-5 diphenyl-3,4 pyrrole (106919-97-5) + N-p.dimethylaminophenyl-2 methyl-5 diphenyl-3,4 pyrrole (106919-96-4)

Guidance literature:

In benzene; for 6h; Heating;

DOI:10.1016/S0040-4020(01)87354-3

upstream raw materials:

N-p.dimethylaminophenyl methyl-5 diphenyl-3,4 pyrrolecarbaldehyde-2

2,5-dimethyl-3,4-diphenylcyclopenta-2,4-dione dimer

p-dimethylaminonitrosobenzene

N-p.dimethylaminophenyl-2 methyl-5 diphenyl-3,4 pyrrole

Downstream raw materials:

N-p.dimethylaminophenyl-2 methyl-5 diphenyl-3,4 pyrrole

N-p.dimethylaminophenyl dimethyl-2,5 diphenyl-3,4 pyrrole

N-p.dimethylaminophenyl methyl-5 diphenyl-3,4 pyrrolecarbaldehyde-2

N-N'-bis(p.dimethylaminophenyl) methyl-5 diphenyl-3,4 pyrrolecarboxamide-2

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