C₂₆⁽¹³⁾CH₃₂O₅

Base Information

Chemical Name:C₂₆⁽¹³⁾CH₃₂O₅
CAS No.:838902-45-7
Molecular Formula:C₂₇H₃₂O₅
Molecular Weight:437.537
Hs Code.:

C<sub>26</sub><sup>(13)</sup>CH<sub>32</sub>O<sub>5</sub>

Synonyms:C₂₆⁽¹³⁾CH₃₂O₅

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Chemical Property of C₂₆⁽¹³⁾CH₃₂O₅

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Technology Process of C₂₆⁽¹³⁾CH₃₂O₅

There total 6 articles about C₂₆⁽¹³⁾CH₃₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 838902-43-5
L-lyxo-hex-1-[1-13C]enitol

: 838902-44-6
C₂₆⁽¹³⁾CH₃₂O₅

: 838902-45-7
C₂₆⁽¹³⁾CH₃₂O₅

Guidance literature:: With osmium(VIII) oxide; N-methyl-2-indolinone; In water; tert-butyl alcohol; at 0 ℃;
DOI:10.1016/j.tetlet.2004.11.073

Reference yield:

: 92622-02-1
1,2,3,4-pentanetetrol

: 838902-45-7
C₂₆⁽¹³⁾CH₃₂O₅

Guidance literature:: Multi-step reaction with 6 steps

1: 90 percent / pyridine / 1 h / 55 °C

2: 95 percent / NaH / dimethylformamide / 0 °C

3: 95 percent / aq. AcOH / 0.5 h / 50 °C

4: 100 percent / trichloroisocyanuric acid; 2,2,6,6-tetramethyl-1-piperidinyloxy radical / CH₂Cl₂ / 0 °C

5: 71 percent / n-BuLi / hexane; tetrahydrofuran / -20 °C

6: 88 percent / OsO₄; NMO / 2-methyl-propan-2-ol; H₂O / 0 °C

With pyridine; 2,2,6,6-tetramethyl-piperidine-N-oxyl; osmium(VIII) oxide; n-butyllithium; N-methyl-2-indolinone; trichloroisocyanuric acid; sodium hydride; acetic acid; In tetrahydrofuran; hexane; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 5: Wittig reaction;
DOI:10.1016/j.tetlet.2004.11.073

Reference yield:

: 838902-42-4
(2R,3R,4S)-2,3,4-Tris-benzyloxy-pentanal

: 838902-45-7
C₂₆⁽¹³⁾CH₃₂O₅

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / n-BuLi / hexane; tetrahydrofuran / -20 °C

2: 88 percent / OsO₄; NMO / 2-methyl-propan-2-ol; H₂O / 0 °C

With osmium(VIII) oxide; n-butyllithium; N-methyl-2-indolinone; In tetrahydrofuran; hexane; water; tert-butyl alcohol; 1: Wittig reaction;
DOI:10.1016/j.tetlet.2004.11.073