Technology Process of C38H51O4SiN
There total 5 articles about C38H51O4SiN which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
n-butyllithium;
In
tetrahydrofuran; hexane;
at -78 ℃;
DOI:10.1021/ol070517g
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 90 percent / lithium hydroxide monohydrate / tetrahydrofuran; methanol; H2O / 5 h / 20 °C
2: oxalyl chloride / benzene; dimethylformamide / 4 h / 20 °C
3: 92 percent / butyllithium / tetrahydrofuran; hexane / -78 °C
With
lithium hydroxide; n-butyllithium; oxalyl dichloride;
In
tetrahydrofuran; methanol; hexane; water; N,N-dimethyl-formamide; benzene;
DOI:10.1021/ol070517g
- Guidance literature:
-
Multi-step reaction with 5 steps
1: H2SO4 / benzene / 12 h / Heating
2: 10.3 g / 4-(dimethylamino)pyridine; triethylamine / CH2Cl2 / 0 - 20 °C
3: 90 percent / lithium hydroxide monohydrate / tetrahydrofuran; methanol; H2O / 5 h / 20 °C
4: oxalyl chloride / benzene; dimethylformamide / 4 h / 20 °C
5: 92 percent / butyllithium / tetrahydrofuran; hexane / -78 °C
With
dmap; lithium hydroxide; n-butyllithium; oxalyl dichloride; sulfuric acid; triethylamine;
In
tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; benzene;
DOI:10.1021/ol070517g