N-((1H-pyrrol-2-yl)methylene)-2-(3,5-dimethyl-1H-pyrazol-1-yl)benzenamine

Base Information

Chemical Name:N-((1H-pyrrol-2-yl)methylene)-2-(3,5-dimethyl-1H-pyrazol-1-yl)benzenamine
CAS No.:1313759-41-9
Molecular Formula:C₁₆H₁₆N₄
Molecular Weight:264.33
Hs Code.:

Synonyms:N-((1H-pyrrol-2-yl)methylene)-2-(3,5-dimethyl-1H-pyrazol-1-yl)benzenamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-((1H-pyrrol-2-yl)methylene)-2-(3,5-dimethyl-1H-pyrazol-1-yl)benzenamine

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Technology Process of N-((1H-pyrrol-2-yl)methylene)-2-(3,5-dimethyl-1H-pyrazol-1-yl)benzenamine

There total 1 articles about N-((1H-pyrrol-2-yl)methylene)-2-(3,5-dimethyl-1H-pyrazol-1-yl)benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1003-29-8,254729-95-8
2-pyrrole aldehyde

: 60418-47-5
2-(3,5-dimethyl-1H-pyrazol-1-yl)benzenamine

: 1313759-41-9
N-((1H-pyrrol-2-yl)methylene)-2-(3,5-dimethyl-1H-pyrazol-1-yl)benzenamine

Guidance literature:: With formic acid; In toluene; for 6h; Molecular sieve; Reflux;
DOI:10.1016/j.jorganchem.2011.04.028

Reference yield: 74.0%

: 1313759-41-9
N-((1H-pyrrol-2-yl)methylene)-2-(3,5-dimethyl-1H-pyrazol-1-yl)benzenamine

: 557-20-0
diethylzinc

: 1313759-43-1
Zn(N-((1H-pyrrol-2-yl)methylene)-2-(3,5-dimethyl-1H-pyrazol-1-yl)benzeneamine(-1H))

Guidance literature:: In hexane; toluene; to stirred soln. of benzenamine deriv. in toluene, hexane soln. of ZnEt2added dropwise at 0°C; mixt. warmed to room temp, stirred overni ght; solvent removed in vacuo; residue dissolved in Et2O, filtered, filtrate concd.; elem. anal.;
DOI:10.1016/j.jorganchem.2011.04.028

Reference yield: 63.0%

: 1313759-41-9
N-((1H-pyrrol-2-yl)methylene)-2-(3,5-dimethyl-1H-pyrazol-1-yl)benzenamine

: 75-24-1
trimethylaluminum

: AlMe(N-((1H-pyrrol-2-yl)methylene)-2-(3,5-dimethyl-1H-pyrazol-1-yl)benzeneamine(-1H))*Et₂O

Guidance literature:: In hexane; toluene; to stirred soln. of benzenamine deriv. in toluene, hexane soln. of AlMe3added at room temp.; stirred overnight; solvent removed in vacuo; residue dissolved in Et2O, filtered, filtrate concd.; elem. anal.;
DOI:10.1016/j.jorganchem.2011.04.028