3-<2'-(β-N-Methylaminoethyl)-4',5'-dimethoxyphenyl>-6,7-dimethoxyisochroman

Base Information

Chemical Name:3-<2'-(β-N-Methylaminoethyl)-4',5'-dimethoxyphenyl>-6,7-dimethoxyisochroman
CAS No.:90601-55-1
Molecular Formula:C₂₂H₂₉NO₅
Molecular Weight:387.476
Hs Code.:

Synonyms:3-<2'-(β-N-Methylaminoethyl)-4',5'-dimethoxyphenyl>-6,7-dimethoxyisochroman

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Chemical Property of 3-<2'-(β-N-Methylaminoethyl)-4',5'-dimethoxyphenyl>-6,7-dimethoxyisochroman

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Technology Process of 3-<2'-(β-N-Methylaminoethyl)-4',5'-dimethoxyphenyl>-6,7-dimethoxyisochroman

There total 3 articles about 3-<2'-(β-N-Methylaminoethyl)-4',5'-dimethoxyphenyl>-6,7-dimethoxyisochroman which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 90601-57-3
3-<2'-(β-N-2,2,2-Trichloroethoxycarbonyl-N-methyl-aminoethyl)-4',5'-dimethoxyphenyl>-6,7-dimethoxyisochroman

: 90601-55-1
3-<2'-(β-N-Methylaminoethyl)-4',5'-dimethoxyphenyl>-6,7-dimethoxyisochroman

Guidance literature:: With acetic acid; zinc; In 1,4-dioxane; for 4h; Ambient temperature;
DOI:10.1002/ardp.19843170512

Reference yield: 62.0%

: 90601-58-4
3-<2'-(β-N-Benzyloxycarbonyl-N-methyl-aminoethyl)-4',5'-dimethoxyphenyl>-6,7-dimethoxyisochroman

: 90601-55-1
3-<2'-(β-N-Methylaminoethyl)-4',5'-dimethoxyphenyl>-6,7-dimethoxyisochroman

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 1h;
DOI:10.1002/ardp.19843170512

Reference yield:

: 50461-20-6
6'-Hydroxymethyl-laudanosine

: 90601-55-1
3-<2'-(β-N-Methylaminoethyl)-4',5'-dimethoxyphenyl>-6,7-dimethoxyisochroman

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / 15percent aq. KOH / CHCl₃; diethyl ether / 4 h / Heating

2: 62 percent / H₂ / 10percent Pd/C / ethanol / 1 h

With potassium hydroxide; hydrogen; palladium on activated charcoal; In diethyl ether; ethanol; chloroform;
DOI:10.1002/ardp.19843170512