N-(1-chloro-2-oxo-2-phenylethyl)-N-(4-methoxyphenyl)-3-<oxy>butanamide

Base Information

Chemical Name:N-(1-chloro-2-oxo-2-phenylethyl)-N-(4-methoxyphenyl)-3-<oxy>butanamide
CAS No.:122358-08-1
Molecular Formula:C₂₈H₄₀ClNO₄Si
Molecular Weight:518.168
Hs Code.:

N-(1-chloro-2-oxo-2-phenylethyl)-N-(4-methoxyphenyl)-3-<<tris(1-methylethyl)silyl>oxy>butanamide

Synonyms:N-(1-chloro-2-oxo-2-phenylethyl)-N-(4-methoxyphenyl)-3-<oxy>butanamide

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Chemical Property of N-(1-chloro-2-oxo-2-phenylethyl)-N-(4-methoxyphenyl)-3-<oxy>butanamide

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Technology Process of N-(1-chloro-2-oxo-2-phenylethyl)-N-(4-methoxyphenyl)-3-<oxy>butanamide

There total 4 articles about N-(1-chloro-2-oxo-2-phenylethyl)-N-(4-methoxyphenyl)-3-<oxy>butanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 113628-33-4,62558-62-7
2-(4-methoxyphenylimino)-1-phenylethanone

: 118990-83-3,122358-04-7
(3R)-(-)-3-<oxy>butanoyl chloride

: 122358-08-1
N-(1-chloro-2-oxo-2-phenylethyl)-N-(4-methoxyphenyl)-3-<oxy>butanamide

Guidance literature:: In dichloromethane; at -20 ℃; for 16h;
DOI:10.1021/jo00277a011

Reference yield:

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 122358-08-1
N-(1-chloro-2-oxo-2-phenylethyl)-N-(4-methoxyphenyl)-3-<oxy>butanamide

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / 2,6-lutidine / 3 h / Ambient temperature

2: 98.3 percent / LiOH / tetrahydrofuran / 40 h / Ambient temperature

3: 88.7 percent / oxalyl chloride / CH₂Cl₂ / 2.5 h / Ambient temperature

4: 38 percent / CH₂Cl₂ / 16 h / -20 °C

With 2,6-dimethylpyridine; lithium hydroxide; oxalyl dichloride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00277a011

Reference yield:

: 118990-82-2,122358-10-5
3(R)-<oxy>butanoic acid

: 122358-08-1
N-(1-chloro-2-oxo-2-phenylethyl)-N-(4-methoxyphenyl)-3-<oxy>butanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 88.7 percent / oxalyl chloride / CH₂Cl₂ / 2.5 h / Ambient temperature

2: 38 percent / CH₂Cl₂ / 16 h / -20 °C

With oxalyl dichloride; In dichloromethane;
DOI:10.1021/jo00277a011