Technology Process of C19H33NO3Si
There total 5 articles about C19H33NO3Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
methanol;
at 0 ℃;
for 1h;
DOI:10.1021/ol070855h
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: NaHMDS / diethyl ether / 0.67 h / -78 °C
1.2: 78 percent / diethyl ether / 1 h / -78 °C
2.1: 83 percent / trifluoroacetic acid / methanol / 1 h / 0 °C
With
sodium hexamethyldisilazane; trifluoroacetic acid;
In
methanol; diethyl ether;
DOI:10.1021/ol070855h
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triethylamine / CH2Cl2 / 3 h / 0 °C
2.1: 87 percent / Ti(OEt)4 / CH2Cl2 / 5 h / 40 °C
3.1: NaHMDS / diethyl ether / 0.67 h / -78 °C
3.2: 78 percent / diethyl ether / 1 h / -78 °C
4.1: 83 percent / trifluoroacetic acid / methanol / 1 h / 0 °C
With
titanium(IV) tetraethanolate; sodium hexamethyldisilazane; triethylamine; trifluoroacetic acid;
In
methanol; diethyl ether; dichloromethane;
DOI:10.1021/ol070855h