methyl 4-azido-5,7-O-benzylidene-6-O-tert-butyldimethylsilyl-2,3,4-trideoxy-D-gulo-oct-2-enoate

Base Information

Chemical Name:methyl 4-azido-5,7-O-benzylidene-6-O-tert-butyldimethylsilyl-2,3,4-trideoxy-D-gulo-oct-2-enoate
CAS No.:874350-77-3
Molecular Formula:C₂₂H₃₃N₃O₆Si
Molecular Weight:463.606
Hs Code.:

Synonyms:methyl 4-azido-5,7-O-benzylidene-6-O-tert-butyldimethylsilyl-2,3,4-trideoxy-D-gulo-oct-2-enoate

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Chemical Property of methyl 4-azido-5,7-O-benzylidene-6-O-tert-butyldimethylsilyl-2,3,4-trideoxy-D-gulo-oct-2-enoate

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Technology Process of methyl 4-azido-5,7-O-benzylidene-6-O-tert-butyldimethylsilyl-2,3,4-trideoxy-D-gulo-oct-2-enoate

There total 1 articles about methyl 4-azido-5,7-O-benzylidene-6-O-tert-butyldimethylsilyl-2,3,4-trideoxy-D-gulo-oct-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₂₉N₃O₅Si

: 1779-58-4
(methyloxycarbonylmethyl)triphenylphosphonium bromide

: 874350-77-3
methyl 4-azido-5,7-O-benzylidene-6-O-tert-butyldimethylsilyl-2,3,4-trideoxy-D-gulo-oct-2-enoate

Guidance literature:: (methyloxycarbonylmethyl)triphenylphosphonium bromide; With sodium hydroxide; In dichloromethane; water; for 0.0833333h;

C₁₉H₂₉N₃O₅Si; In 1,4-dioxane; at 20 ℃;

Reference yield: 57.0%

: 874350-77-3
methyl 4-azido-5,7-O-benzylidene-6-O-tert-butyldimethylsilyl-2,3,4-trideoxy-D-gulo-oct-2-enoate

: 874350-84-2
methyl 4-azido-5,7-O-benzylidene-8-O-tert-butyldimethylsilyl-4-deoxy-D-threo-D-altro-octonate

Guidance literature:: With potassium hexacyanoferrate (III); potassium osmate(VI); methanesulfonamide; potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; In dichloromethane; water; tert-butyl alcohol; at 0 ℃; for 4.16h;

Reference yield: 48.0%

: 874350-77-3
methyl 4-azido-5,7-O-benzylidene-6-O-tert-butyldimethylsilyl-2,3,4-trideoxy-D-gulo-oct-2-enoate

: 874350-78-4
4-azido-5,7-O-benzylidene-8-O-tert-butyldimethylsilyl-4-deoxy-D-gluco-D-threo-octono-γ-lactone

Guidance literature:: With (DHQ)2PHAL; potassium hexacyanoferrate (III); potassium osmate(VI); methanesulfonamide; potassium carbonate; In water; tert-butyl alcohol; at 0 - 20 ℃;