Technology Process of C47H66O10Si
There total 13 articles about C47H66O10Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C47H64O9Si;
With
borane-THF;
at 0 - 20 ℃;
With
sodium perborate;
In
tetrahydrofuran; water;
Further stages.;
Heating;
DOI:10.1016/j.bmcl.2006.09.004
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 97 percent / KOH / methanol; tetrahydrofuran; H2O / Heating
2.1: EDC*HCl; DMAP; CSA / CH2Cl2 / Heating
3.1: H2O; TsOH / methanol / 20 °C
4.1: 2,6-lutidine / dimethylformamide / 0 °C
5.1: Cp2Ti[P(OEt)3]2 / tetrahydrofuran / 20 °C
6.1: BH3*THF / 0 - 20 °C
6.2: NaBO3 / H2O; tetrahydrofuran / Heating
With
2,6-dimethylpyridine; dmap; potassium hydroxide; borane-THF; titanocene(II) triethylphosphite complex; camphor-10-sulfonic acid; water; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2006.09.004
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: H2O; TsOH / methanol / 20 °C
2.1: 2,6-lutidine / dimethylformamide / 0 °C
3.1: Cp2Ti[P(OEt)3]2 / tetrahydrofuran / 20 °C
4.1: BH3*THF / 0 - 20 °C
4.2: NaBO3 / H2O; tetrahydrofuran / Heating
With
2,6-dimethylpyridine; borane-THF; titanocene(II) triethylphosphite complex; water; toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2006.09.004
