(NH₃)5CoO(COCH(CH₂C₆H₅)NH)2COC₅H₄NOs(NH₃)5⁽⁵⁺⁾*5BF₄^(1-)=(NH₃)5CoO(COCH(CH₂C₆H₅)NH)2COC₅H₄NOs(NH₃)5(BF₄)5

Base Information

• Chemical Name: (NH₃)5CoO(COCH(CH₂C₆H₅)NH)2COC₅H₄NOs(NH₃)5⁽⁵⁺⁾*5BF₄^(1-)=(NH₃)5CoO(COCH(CH₂C₆H₅)NH)2COC₅H₄NOs(NH₃)5(BF₄)5
• CAS No.: 98466-64-9
• Molecular Formula: 5BF₄*C₂₄H₅₂CoN₁₃O₄Os
• Molecular Weight: 1269.98

Synonyms:(NH₃)5CoO(COCH(CH₂C₆H₅)NH)2COC₅H₄NOs(NH₃)5⁽⁵⁺⁾*5BF₄^(1-)=(NH₃)5CoO(COCH(CH₂C₆H₅)NH)2COC₅H₄NOs(NH₃)5(BF₄)5

Chemical Property of (NH₃)5CoO(COCH(CH₂C₆H₅)NH)2COC₅H₄NOs(NH₃)5⁽⁵⁺⁾*5BF₄^(1-)=(NH₃)5CoO(COCH(CH₂C₆H₅)NH)2COC₅H₄NOs(NH₃)5(BF₄)5

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Technology Process of (NH₃)5CoO(COCH(CH₂C₆H₅)NH)2COC₅H₄NOs(NH₃)5⁽⁵⁺⁾*5BF₄^(1-)=(NH₃)5CoO(COCH(CH₂C₆H₅)NH)2COC₅H₄NOs(NH₃)5(BF₄)5

There total 1 articles about (NH₃)5CoO(COCH(CH₂C₆H₅)NH)2COC₅H₄NOs(NH₃)5⁽⁵⁺⁾*5BF₄^(1-)=(NH₃)5CoO(COCH(CH₂C₆H₅)NH)2COC₅H₄NOs(NH₃)5(BF₄)5 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetrafluoroboric acid + (NH3)5CoO(COCH(CH2C6H5)NH)2COC5H4NOs(NH3)5(5+)*5CF3COO(1-)=(NH3)5CoO(COCH(CH2C6H5)NH)2COC5H4NOs(NH3)5(CF3COO)5 → (NH3)5CoO(COCH(CH2C6H5)NH)2COC5H4NOs(NH3)5(5+)*5BF4(1-)=(NH3)5CoO(COCH(CH2C6H5)NH)2COC5H4NOs(NH3)5(BF4)5 (98466-64-9)

Guidance literature:

In trifluoroacetic acid; HBF4 was added to a soln. of binuclear complex in CF3COOH; ethanol and ether were added, ppt. collected, washed with ether, redissolved in water, applied to a Bio-Gel P-2 column, the main band was collected, concd. to dryness by rotary evapn.;

DOI:10.1021/ja00311a035

Reference yield:

(NH3)5CoO(COCH(CH2C6H5)NH)2COC5H4NOs(NH3)5(5+)*5BF4(1-)=(NH3)5CoO(COCH(CH2C6H5)NH)2COC5H4NOs(NH3)5(BF4)5 (98466-64-9) → HO(COCH(CH2C6H5)NH)2COC5H4NOs(NH3)5(3+)

Guidance literature:

With Me₂COH radical or CO₂ radical anion; In water; isopropyl alcohol; trifluoroacetic acid; byproducts: Co(2+), NH4(1+); other Radiation; a soln. of OsCo-complex in 0.1 M CF3COOH - 0.1 M i-PrOH was degassed and subjected to pulse radiolysis, reaction was monitored by UV spectroscopy; electron transfer rate const. (formation of Os(III)-L-Co(II) intermediate) and activation parameters given; Kinetics;

DOI:10.1021/ja00311a035

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