allyl 2-acetamido-4-O-(6-O-benzoyl-2,3-di-O-benzyl-β-D-galactopyranosyl)-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Base Information

• Chemical Name: allyl 2-acetamido-4-O-(6-O-benzoyl-2,3-di-O-benzyl-β-D-galactopyranosyl)-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside
• CAS No.: 88509-77-7
• Molecular Formula: C₅₂H₅₇NO₁₂
• Molecular Weight: 888.024

Synonyms:allyl 2-acetamido-4-O-(6-O-benzoyl-2,3-di-O-benzyl-β-D-galactopyranosyl)-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Chemical Property of allyl 2-acetamido-4-O-(6-O-benzoyl-2,3-di-O-benzyl-β-D-galactopyranosyl)-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Chemical Property:

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Technology Process of allyl 2-acetamido-4-O-(6-O-benzoyl-2,3-di-O-benzyl-β-D-galactopyranosyl)-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

There total 1 articles about allyl 2-acetamido-4-O-(6-O-benzoyl-2,3-di-O-benzyl-β-D-galactopyranosyl)-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

benzoyl cyanide (613-90-1) + allyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-(2,3-di-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranoside (88509-76-6) → allyl 2-acetamido-4-O-(6-O-benzoyl-2,3-di-O-benzyl-β-D-galactopyranosyl)-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside (88509-77-7)

Guidance literature:

With pyridine; methanol; In dichloromethane; for 5h; Ambient temperature;

DOI:10.1016/0008-6215(83)88331-1

Reference yield: 78.0%

(2R,3S,4S,5R,6R)-3,4,5-Tris-benzyloxy-2-benzyloxymethyl-6-chloro-tetrahydro-pyran (4291-68-3,25320-59-6,41110-63-8,67068-83-1,67773-44-8,69237-96-3,92470-93-4,93601-69-5,113829-62-2) + allyl 2-acetamido-4-O-(6-O-benzoyl-2,3-di-O-benzyl-β-D-galactopyranosyl)-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside (88509-77-7) → allyl 2-acetamido-4-O-<6-O-benzoyl-2,3-di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-β-D-galactopyranosyl>-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside (88509-78-8) + allyl 2-acetamido-4-O-<6-O-benzoyl-2,3-di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-β-D-galactopyranosyl>-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside (88509-78-8)

Guidance literature:

With 2,4,6-trimethyl-pyridine; 4 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; Title compound not separated from byproducts; 1.) 0.5 h, 2.) 5 d;

DOI:10.1016/0008-6215(83)88331-1

upstream raw materials:

benzoyl cyanide

allyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-(2,3-di-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Downstream raw materials:

allyl 2-acetamido-4-O-<6-O-benzoyl-2,3-di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-β-D-galactopyranosyl>-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

allyl 2-acetamido-4-O-<6-O-benzoyl-2,3-di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-β-D-galactopyranosyl>-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

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