ACETONEMETHYLHYDRAZONE

Base Information

• Chemical Name: ACETONEMETHYLHYDRAZONE
• CAS No.: 5771-02-8
• Molecular Formula: C4H10N2
• Molecular Weight: 86.1368
• Mol file: 5771-02-8.mol

Synonyms:acetone 1-methylhydrazone;Me2C=N-NHMe;1-isopropylidene-2-methylhydrazine;N-isopropiylidene-N'-methylhydrazine;N-isopropylidene-N'-methylhydrazine;2-Propanone,methylhydrazone;N'-methyl-N-isopropylidenehydrazine;Acetone methylhydrazone;

Chemical Property of ACETONEMETHYLHYDRAZONE

Chemical Property:

• Vapor Pressure: 43.4mmHg at 25°C
• Boiling Point: 96.5°C at 760 mmHg
• Flash Point: 12.2°C
• PSA: 24.39000
• Density: 0.83g/cm³
• LogP: 0.99250

Purity/Quality:

99% ^*data from raw suppliers

Acetone N-methylhydrazone ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ACETONEMETHYLHYDRAZONE

There total 2 articles about ACETONEMETHYLHYDRAZONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-[[(4-methoxyphenyl)methylhydrazono]methyl]-1,3,3-trimethyl-3H-indolium methyl sulfate (54060-92-3) → 2-methyllactic acid (594-61-6) + malonic acid (141-82-2) + N-isopropylidene-N'-methylhydrazine (5771-02-8) + 2-Pentanone (107-87-9)

Guidance literature:

With ferrous(II) sulfate heptahydrate; dipotassium peroxodisulfate; sulfuric acid; In water; at 70 ℃; for 8h; pH=3.5; Concentration; Temperature; Time;

DOI:10.14233/ajchem.2013.14941

Reference yield:

2-(Phenylazo)-2-(methylazo)propane → methane (34557-54-5,27936-85-2) + N-isopropylidene-N'-methylhydrazine (5771-02-8) + acetone phenylhydrazone (103-02-6)

Guidance literature:

In xylene; at 30.5 ℃; Kinetics; Thermodynamic data; temp. range 30.5-41.2 deg C, ΔH(excit.), ΔS(excit.), ΔG(excit.);

DOI:10.1021/jo00100a028

Reference yield: 92.0%

N-isopropylidene-N'-methylhydrazine (5771-02-8) + methyl benzenecarbimidothioate hydroiodide (41981-24-2) → C11H15N3*HI (84044-62-2)

Guidance literature:

DOI:10.1007/BF00503615

upstream raw materials:

2-[[(4-methoxyphenyl)methylhydrazono]methyl]-1,3,3-trimethyl-3H-indolium methyl sulfate

Downstream raw materials:

2-Methylazo-propan-2-ol-acetat

(3E)-4-(2-Isopropyliden-1-methylhydrazino)-3-buten-2-on

(2E)-3-(2-Isopropyliden-1-methylhydrazino)acrylsaeure-methylester

Aceton<4-(2.6-dimethylphenyl)-2-methylthiosemicarbazon>