Re(OC(CH₃)2)Cl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={Re(OC(CH₃)2)Cl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4

Base Information

• Chemical Name: Re(OC(CH₃)2)Cl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={Re(OC(CH₃)2)Cl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4
• CAS No.: 130327-36-5
• Molecular Formula: C₁₂H₂₇Cl₂N₃ORe*C₂₄H₂₀B
• Molecular Weight: 805.713

Synonyms:Re(OC(CH₃)2)Cl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={Re(OC(CH₃)2)Cl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4

Chemical Property of Re(OC(CH₃)2)Cl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={Re(OC(CH₃)2)Cl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4

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Technology Process of Re(OC(CH₃)2)Cl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={Re(OC(CH₃)2)Cl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4

There total 1 articles about Re(OC(CH₃)2)Cl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={Re(OC(CH₃)2)Cl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

Re(OP(C6H5)3)Cl2((CH3)NCH2CH2)3(1+)*B(C6H5)4(1-)={Re(OP(C6H5)3)Cl2((CH3)NCH2CH2)3}B(C6H5)4 (130327-30-9) → Re(OC(CH3)2)Cl2((CH3)NCH2CH2)3(1+)*B(C6H5)4(1-)={Re(OC(CH3)2)Cl2((CH3)NCH2CH2)3}B(C6H5)4 (130327-36-5)

Guidance literature:

With acetone; In acetone; byproducts: OP(C6H5)3; Schlenk or vacuum-line techniques, N2-glovebox, ambient temp.; addn. of acetone to Re-complex, soln. stirred (3 d); concn. (to 5 ml), addn. of Et2O, pptn., filtration, washed (Et2O), evapn.;

Reference yield: 41.0%

Re(OC(CH3)2)Cl2((CH3)NCH2CH2)3(1+)*B(C6H5)4(1-)={Re(OC(CH3)2)Cl2((CH3)NCH2CH2)3}B(C6H5)4 (130327-36-5) → Re(C5H5N)Cl2((CH3)NCH2CH2)3(1+)*B(C6H5)4(1-)={Re(C5H5N)Cl2((CH3)NCH2CH2)3}B(C6H5)4 (130327-38-7)

Guidance literature:

With pyridine; In acetone; byproducts: acetone; Schlenk or vacuum-line techniques, N2-glovebox, ambient temp.; addn. of pyridine to Re-complex in acetone, soln. stirred (4 d); evapn. (to dryness), soln. with minimum amount of acetone, filtration, addn. of Et2O, pptn., filtration, washed (Et2O);

Reference yield:

Re(OC(CH3)2)Cl2((CH3)NCH2CH2)3(1+)*B(C6H5)4(1-)={Re(OC(CH3)2)Cl2((CH3)NCH2CH2)3}B(C6H5)4 (130327-36-5) → Re(OC(CD3)2)Cl2((CH3)NCH2CH2)3(1+)*B(C6H5)4(1-)={Re(OC(CD3)2)Cl2((CH3)NCH2CH2)3}B(C6H5)4

Guidance literature:

With OC(CD₃)3; In [⁽²⁾H₆]acetone; schlenk or vacuum-line techniques, N2-glovebox, ambient temp.; readily exchanged;

upstream raw materials:

Re(OP(C₆H₅)3)Cl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={Re(OP(C₆H₅)3)Cl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4

Downstream raw materials:

Re(C₅H₅N)Cl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={Re(C₅H₅N)Cl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4

ReOCl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={ReOCl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4

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