4-Acetoxy-3-[1-phenyl-meth-(Z)-ylidene]-cyclopenta-1,4-dienecarboxylic acid methyl ester

Base Information

Chemical Name:4-Acetoxy-3-[1-phenyl-meth-(Z)-ylidene]-cyclopenta-1,4-dienecarboxylic acid methyl ester
CAS No.:83406-73-9
Molecular Formula:C₁₆H₁₄O₄
Molecular Weight:270.285
Hs Code.:

Synonyms:4-Acetoxy-3-[1-phenyl-meth-(Z)-ylidene]-cyclopenta-1,4-dienecarboxylic acid methyl ester

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Chemical Property of 4-Acetoxy-3-[1-phenyl-meth-(Z)-ylidene]-cyclopenta-1,4-dienecarboxylic acid methyl ester

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Technology Process of 4-Acetoxy-3-[1-phenyl-meth-(Z)-ylidene]-cyclopenta-1,4-dienecarboxylic acid methyl ester

There total 2 articles about 4-Acetoxy-3-[1-phenyl-meth-(Z)-ylidene]-cyclopenta-1,4-dienecarboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 108-24-7
acetic anhydride

: 83406-57-9
2-[(E)-3-Phenyl-prop-2-en-(Z)-ylidene]-succinic acid 1-methyl ester

: 83406-73-9
4-Acetoxy-3-[1-phenyl-meth-(Z)-ylidene]-cyclopenta-1,4-dienecarboxylic acid methyl ester

Guidance literature:: With sodium acetate; for 3h; Heating;

Reference yield:

: 106-65-0
Dimethyl succinate

: 83406-73-9
4-Acetoxy-3-[1-phenyl-meth-(Z)-ylidene]-cyclopenta-1,4-dienecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / K/tert-butanol / 2-methyl-propan-2-ol / 1 h / 70 - 80 °C

2: 70 percent / CH₃COONa / 3 h / Heating

With sodium acetate; tert-butyl alcohol; In tert-butyl alcohol;