beta-Ethyl-4-methoxy-alpha-(4-methoxyphenyl)-benzenepropanol

Base Information

• Chemical Name: beta-Ethyl-4-methoxy-alpha-(4-methoxyphenyl)-benzenepropanol
• CAS No.: 71526-43-7
• Molecular Formula: C19H24 O3
• Molecular Weight: 0
• Mol file: 71526-43-7.mol

Synonyms:beta-Ethyl-4-methoxy-alpha-(4-methoxyphenyl)-benzenepropanol

Chemical Property of beta-Ethyl-4-methoxy-alpha-(4-methoxyphenyl)-benzenepropanol

Chemical Property:

• Vapor Pressure: 1.15E-08mmHg at 25°C
• Boiling Point: 444.1°C at 760 mmHg
• Flash Point: 222.4°C
• PSA: 38.69000
• Density: 1.076g/cm³
• LogP: 4.00610

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of beta-Ethyl-4-methoxy-alpha-(4-methoxyphenyl)-benzenepropanol

There total 3 articles about beta-Ethyl-4-methoxy-alpha-(4-methoxyphenyl)-benzenepropanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

2-(4-methoxybenzyl)-1-(4-methoxyphenyl)butan-1-one (71526-42-6) → 2-(4-Methoxy-benzyl)-1-(4-methoxy-phenyl)-butan-1-ol (71526-43-7)

Guidance literature:

With sodium tetrahydroborate; In methanol; Heating;

Reference yield:

1-(4-Methoxy-phenyl)-2-[1-(4-methoxy-phenyl)-meth-(Z)-ylidene]-butan-1-one (71526-41-5,71526-40-4) → 2-(4-Methoxy-benzyl)-1-(4-methoxy-phenyl)-butan-1-ol (71526-43-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / H₂ / 10percent Pd/C / ethyl acetate / 760 Torr / Ambient temperature

2: 83 percent / NaBH₄ / methanol / Heating

With sodium tetrahydroborate; hydrogen; palladium on activated charcoal; In methanol; ethyl acetate;

Reference yield:

→ 2-(4-Methoxy-benzyl)-1-(4-methoxy-phenyl)-butan-1-ol (71526-43-7)

Guidance literature:

Chalcon-Gem. 3a,b, H2;

upstream raw materials:

2-(4-methoxybenzyl)-1-(4-methoxyphenyl)butan-1-one

1-(4-Methoxy-phenyl)-2-[1-(4-methoxy-phenyl)-meth-(Z)-ylidene]-butan-1-one

Downstream raw materials:

Acetic acid 4-[2-(4-methoxy-benzyl)-1-(4-methoxy-phenyl)-butyl]-phenyl ester

1-(2-{4-[2-(4-Methoxy-benzyl)-1-(4-methoxy-phenyl)-butyl]-phenoxy}-ethyl)-pyrrolidine

1-(o-hydroxyphenyl)-2-(p-methoxybenzyl)-1-(p-methoxyphenyl)butane

1-(p-hydroxyphenyl)-2-(p-methoxybenzyl)-1-(p-methoxyphenyl)butane

Refernces