2-methyl-4aβ-(3-methoxyphenyl)-1,2,3,4,4a,5,6,7,8,8aα-decahydroisoquinoline

Base Information

• Chemical Name: 2-methyl-4aβ-(3-methoxyphenyl)-1,2,3,4,4a,5,6,7,8,8aα-decahydroisoquinoline
• CAS No.: 51605-17-5
• Molecular Formula: C₁₇H₂₅NO
• Molecular Weight: 259.392

Synonyms:2-methyl-4aβ-(3-methoxyphenyl)-1,2,3,4,4a,5,6,7,8,8aα-decahydroisoquinoline

Chemical Property of 2-methyl-4aβ-(3-methoxyphenyl)-1,2,3,4,4a,5,6,7,8,8aα-decahydroisoquinoline

Chemical Property:

Purity/Quality:

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Technology Process of 2-methyl-4aβ-(3-methoxyphenyl)-1,2,3,4,4a,5,6,7,8,8aα-decahydroisoquinoline

There total 2 articles about 2-methyl-4aβ-(3-methoxyphenyl)-1,2,3,4,4a,5,6,7,8,8aα-decahydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(4aS,8aS)-4a-(3-Methoxy-phenyl)-octahydro-isoquinoline-2-carboxylic acid vinyl ester (102538-22-7) → 2-methyl-4aβ-(3-methoxyphenyl)-1,2,3,4,4a,5,6,7,8,8aα-decahydroisoquinoline (51605-17-5)

Guidance literature:

With sodium bis(2-methoxyethoxy)aluminium dihydride; In toluene; at 90 ℃; for 1h;

DOI:10.1021/jm00398a011

Reference yield:

→ 2-methyl-4aβ-(3-methoxyphenyl)-1,2,3,4,4a,5,6,7,8,8aα-decahydroisoquinoline (51605-17-5)

Guidance literature:

d. Octahydroisochinolin (Va), H2, PtO2;

Reference yield: 55.0%

2-methyl-4aβ-(3-methoxyphenyl)-1,2,3,4,4a,5,6,7,8,8aα-decahydroisoquinoline (51605-17-5) → 3-(2-methyl-1,2,3,4,4a,5,6,7,8,8aα-decahydroisoquinolinyl)phenol (51605-18-6)

Guidance literature:

With hydrogen bromide; In acetic acid; for 18h; Heating;

DOI:10.1021/jm00398a011

upstream raw materials:

(4aS,8aS)-4a-(3-Methoxy-phenyl)-octahydro-isoquinoline-2-carboxylic acid vinyl ester

Downstream raw materials:

3-(2-methyl-1,2,3,4,4a,5,6,7,8,8aα-decahydroisoquinolinyl)phenol

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