[1-(3,5-dimethoxy-phenyl)-cyclohexa-2,5-dienyl]-acetic acid methyl ester

Base Information

Chemical Name:[1-(3,5-dimethoxy-phenyl)-cyclohexa-2,5-dienyl]-acetic acid methyl ester
CAS No.:912580-95-1
Molecular Formula:C₁₇H₂₀O₄
Molecular Weight:288.343
Hs Code.:

Synonyms:[1-(3,5-dimethoxy-phenyl)-cyclohexa-2,5-dienyl]-acetic acid methyl ester

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Chemical Property of [1-(3,5-dimethoxy-phenyl)-cyclohexa-2,5-dienyl]-acetic acid methyl ester

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Technology Process of [1-(3,5-dimethoxy-phenyl)-cyclohexa-2,5-dienyl]-acetic acid methyl ester

There total 3 articles about [1-(3,5-dimethoxy-phenyl)-cyclohexa-2,5-dienyl]-acetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 912580-93-9
[1-(3-hydroxy-5-methoxy-phenyl)-cyclohexa-2,5-dienyl]-acetic acid methyl ester

: 77-78-1
dimethyl sulfate

: 912580-95-1
[1-(3,5-dimethoxy-phenyl)-cyclohexa-2,5-dienyl]-acetic acid methyl ester

Guidance literature:: With potassium carbonate; In acetone; at 60 ℃; for 16h;
DOI:10.1021/ol0618353

Reference yield:

: 3-cyclohexa-2,5-dienyl-5-methoxy-phenol

: 912580-95-1
[1-(3,5-dimethoxy-phenyl)-cyclohexa-2,5-dienyl]-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.51 g / tetrahydrofuran; hexane / 0.17 h

2: 80 percent / potassium carbonate / acetone / 16 h / 60 °C

With potassium carbonate; In tetrahydrofuran; hexane; acetone;
DOI:10.1021/ol0618353

Reference yield:

: 55814-99-8
5-methoxy-[1,1′-biphenyl]-3-ol

: 912580-95-1
[1-(3,5-dimethoxy-phenyl)-cyclohexa-2,5-dienyl]-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-BuLi / tetrahydrofuran; hexane / 0.25 h / -78 °C

1.2: 49 percent / ammonia; lithium wire / tetrahydrofuran; hexane / 1 h / Heating

2.1: 1.51 g / tetrahydrofuran; hexane / 0.17 h

3.1: 80 percent / potassium carbonate / acetone / 16 h / 60 °C

With n-butyllithium; potassium carbonate; In tetrahydrofuran; hexane; acetone; 1.2: Birch reduction;
DOI:10.1021/ol0618353