1,3-dimethyl 2-(3-methylbut-2-en-1-yl)-2-(6-(4-nitrophenyl)-6-oxohex-2-yn-1-yl)malonate

Base Information

Chemical Name:1,3-dimethyl 2-(3-methylbut-2-en-1-yl)-2-(6-(4-nitrophenyl)-6-oxohex-2-yn-1-yl)malonate
CAS No.:1392011-68-5
Molecular Formula:C₂₂H₂₅NO₇
Molecular Weight:415.443
Hs Code.:

Synonyms:1,3-dimethyl 2-(3-methylbut-2-en-1-yl)-2-(6-(4-nitrophenyl)-6-oxohex-2-yn-1-yl)malonate

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Chemical Property of 1,3-dimethyl 2-(3-methylbut-2-en-1-yl)-2-(6-(4-nitrophenyl)-6-oxohex-2-yn-1-yl)malonate

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Technology Process of 1,3-dimethyl 2-(3-methylbut-2-en-1-yl)-2-(6-(4-nitrophenyl)-6-oxohex-2-yn-1-yl)malonate

There total 1 articles about 1,3-dimethyl 2-(3-methylbut-2-en-1-yl)-2-(6-(4-nitrophenyl)-6-oxohex-2-yn-1-yl)malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 22731-72-2
1-(4-nitrophenyl)prop-2-en-1-one

: 107473-14-3
dimethyl 2-propargyl-2-prenylmalonate

: 1392011-68-5
1,3-dimethyl 2-(3-methylbut-2-en-1-yl)-2-(6-(4-nitrophenyl)-6-oxohex-2-yn-1-yl)malonate

Guidance literature:: With pyrrolidine; In toluene; at 20 - 60 ℃; for 13h; Inert atmosphere;
DOI:10.1039/c2ob25419k

Reference yield: 88.0%

: 1392011-68-5
1,3-dimethyl 2-(3-methylbut-2-en-1-yl)-2-(6-(4-nitrophenyl)-6-oxohex-2-yn-1-yl)malonate

: 1392011-69-6
dimethyl 7,7-dimethyl-6-(3-(4-nitrophenyl)-3-oxopropyl)bicyclo[3.2.0]hept-5-ene-3,3-dicarboxylate

Guidance literature:: With C₃₄H₄₁AuN₃⁽²⁺⁾*F₆Sb^(1-); In dichloromethane; at 23 ℃; for 12h; Inert atmosphere;
DOI:10.1039/c2ob25419k

Reference yield:

: 1392011-68-5
1,3-dimethyl 2-(3-methylbut-2-en-1-yl)-2-(6-(4-nitrophenyl)-6-oxohex-2-yn-1-yl)malonate

: 1392011-64-1
(Z)-dimethyl 6-((3Z)-3-(2-(2,4-dinitrophenyl)hydrazono)-3-(4-nitrophenyl)propyl)-7,7-dimethylbicyclo[3.2.0]hept-5-ene-3,3-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: C₃₄H₄₁AuN₃⁽²⁺⁾*F₆Sb^(1-) / dichloromethane / 12 h / 23 °C / Inert atmosphere

2.1: sulfuric acid / ethanol; water / 0.17 h / 20 °C / Inert atmosphere

2.2: 0.25 h / 23 °C / Inert atmosphere

With sulfuric acid; C₃₄H₄₁AuN₃⁽²⁺⁾*F₆Sb^(1-); In ethanol; dichloromethane; water;
DOI:10.1039/c2ob25419k