Trifluoro-methanesulfonate2-ethoxycarbonyl-4,6-diphenyl-1-p-tolyl-pyridinium;

Base Information

Chemical Name:Trifluoro-methanesulfonate2-ethoxycarbonyl-4,6-diphenyl-1-p-tolyl-pyridinium;
CAS No.:89409-88-1
Molecular Formula:CF₃O₃S*C₂₇H₂₄NO₂
Molecular Weight:543.563
Hs Code.:

Synonyms:Trifluoro-methanesulfonate2-ethoxycarbonyl-4,6-diphenyl-1-p-tolyl-pyridinium;

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Chemical Property of Trifluoro-methanesulfonate2-ethoxycarbonyl-4,6-diphenyl-1-p-tolyl-pyridinium;

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Technology Process of Trifluoro-methanesulfonate2-ethoxycarbonyl-4,6-diphenyl-1-p-tolyl-pyridinium;

There total 1 articles about Trifluoro-methanesulfonate2-ethoxycarbonyl-4,6-diphenyl-1-p-tolyl-pyridinium; which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 85056-65-1
2-(ethoxycarbonyl)-4,6-diphenylpyrylium trifluoromethanesulphonate

: 106-49-0,12221-03-3
p-toluidine

: 89409-88-1
Trifluoro-methanesulfonate2-ethoxycarbonyl-4,6-diphenyl-1-p-tolyl-pyridinium;

Guidance literature:: In dichloromethane; at 25 ℃; for 4h;
DOI:10.1039/P19830002611

Reference yield: 86.0%

: 89409-88-1
Trifluoro-methanesulfonate2-ethoxycarbonyl-4,6-diphenyl-1-p-tolyl-pyridinium;

: 85574-17-0
1-(p-tolyl)-4,6-diphenylpyridinium-2-carboxylate

Guidance literature:: With sodium hydroxide; at 25 ℃; for 24h;
DOI:10.1039/P19830002611

Reference yield:

: 89409-88-1
Trifluoro-methanesulfonate2-ethoxycarbonyl-4,6-diphenyl-1-p-tolyl-pyridinium;

: 2,4-Diphenyl-1-p-tolyl-6-p-tolylcarbamoyl-pyridinium; chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / aq. NaOH / 24 h / 25 °C

2: 1.) thionyl chloride, pyridine / 1.) CH₂Cl₂, reflux, 15 min, 2.) 75 min, reflux

With pyridine; sodium hydroxide; thionyl chloride;
DOI:10.1039/P19830002611