methyl 3-O-acetyl-2-deoxy-5-O-p-toluenesulfonyl-D-erythro-pentofuranoside

Base Information

Chemical Name:methyl 3-O-acetyl-2-deoxy-5-O-p-toluenesulfonyl-D-erythro-pentofuranoside
CAS No.:62853-11-6
Molecular Formula:C₁₅H₂₀O₇S
Molecular Weight:344.386
Hs Code.:

Synonyms:methyl 3-O-acetyl-2-deoxy-5-O-p-toluenesulfonyl-D-erythro-pentofuranoside

Suppliers and Price of methyl 3-O-acetyl-2-deoxy-5-O-p-toluenesulfonyl-D-erythro-pentofuranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-O-acetyl-2-deoxy-5-O-p-toluenesulfonyl-D-erythro-pentofuranoside

Chemical Property:

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Technology Process of methyl 3-O-acetyl-2-deoxy-5-O-p-toluenesulfonyl-D-erythro-pentofuranoside

There total 4 articles about methyl 3-O-acetyl-2-deoxy-5-O-p-toluenesulfonyl-D-erythro-pentofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 10437-39-5
methyl 2-deoxy-5-O-(p-toluenesulfonyl)-α,β-D-erythro-pentofuranoside

: 108-24-7
acetic anhydride

: 62853-11-6
methyl 3-O-acetyl-2-deoxy-5-O-p-toluenesulfonyl-D-erythro-pentofuranoside

Guidance literature:: With pyridine;
DOI:10.1016/S0008-6215(99)00175-5

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 62853-11-6
methyl 3-O-acetyl-2-deoxy-5-O-p-toluenesulfonyl-D-erythro-pentofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / pyridine / 2 h / 0 - 20 °C

2: 95 percent / pyridine

With pyridine; 1: Tosylation / 2: Acetylation;
DOI:10.1016/S0008-6215(99)00175-5

Reference yield:

: 51255-17-5,51255-18-6,60134-26-1,89577-26-4,96038-80-1,96039-31-5,144301-84-8,144301-85-9
1-O-methyl-2-deoxy-D-ribofuranoside

: 62853-11-6
methyl 3-O-acetyl-2-deoxy-5-O-p-toluenesulfonyl-D-erythro-pentofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / pyridine / 2 h / 0 - 20 °C

2: 95 percent / pyridine

With pyridine; 1: Tosylation / 2: Acetylation;
DOI:10.1016/S0008-6215(99)00175-5