1-methyl-3-(4-hydroxyl-styrenyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Base Information

• Chemical Name: 1-methyl-3-(4-hydroxyl-styrenyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene
• CAS No.: 1201643-14-2
• Molecular Formula: C₁₈H₁₅BF₂N₂O
• Molecular Weight: 324.138

Synonyms:1-methyl-3-(4-hydroxyl-styrenyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Chemical Property of 1-methyl-3-(4-hydroxyl-styrenyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-methyl-3-(4-hydroxyl-styrenyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

There total 4 articles about 1-methyl-3-(4-hydroxyl-styrenyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

1-methyl-3-(4-(2,4-dinitrophenylsulfonyloxy)styrenyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene → 1-methyl-3-(4-hydroxyl-styrenyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1201643-14-2)

Guidance literature:

With thiophenol; triethylamine; In dichloromethane; at 20 ℃; for 0.0833333h;

DOI:10.1039/c004344c

Reference yield: 86.0%

1-methyl-3-(4-(2,4-dinitrophenylsulfonyloxy)styrenyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene + thiophenol (108-98-5) → 1-methyl-3-(4-hydroxyl-styrenyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1201643-14-2)

Guidance literature:

With (C₂H₅)3N; In CH₂Cl₂; mixing C6H5SH, (C2H5)3N, B complex in CH2Cl2 at room temp., storage for 5 min;

DOI:10.1039/c004344c

Reference yield: 47.0%

5,5-difluoro-1,3-dimethyl-5H-4λ4,5λ,4-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinine (154793-49-4) + 4-hydroxy-benzaldehyde (123-08-0,65581-83-1) → 1-methyl-3-(4-hydroxyl-styrenyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1201643-14-2)

Guidance literature:

With pyridine; acetic acid; In toluene; at 90 ℃; for 3h;

DOI:10.1016/j.tet.2015.10.081

upstream raw materials:

thiophenol

5,5-difluoro-1,3-dimethyl-5H-4λ4,5λ,4-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinine

4-hydroxy-benzaldehyde

2-pyrrole aldehyde

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1201643-14-2 1-methyl-3-(4-hydroxyl-styrenyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Send

Send

Metric Ton KG G Pound L ML

Send

Send