{2-cyclohexyl-2-[(2-hydroxy-ethyl)-(2-methanesulfonylamino-benzoyl)-amino]-acetylamino}-acetic acid tert-butyl ester

Base Information

Chemical Name:{2-cyclohexyl-2-[(2-hydroxy-ethyl)-(2-methanesulfonylamino-benzoyl)-amino]-acetylamino}-acetic acid tert-butyl ester
CAS No.:934421-09-7
Molecular Formula:C₂₄H₃₇N₃O₇S
Molecular Weight:511.64
Hs Code.:

{2-cyclohexyl-2-[(2-hydroxy-ethyl)-(2-methanesulfonylamino-benzoyl)-amino]-acetylamino}-acetic acid <i>tert</i>-butyl ester

Synonyms:{2-cyclohexyl-2-[(2-hydroxy-ethyl)-(2-methanesulfonylamino-benzoyl)-amino]-acetylamino}-acetic acid tert-butyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {2-cyclohexyl-2-[(2-hydroxy-ethyl)-(2-methanesulfonylamino-benzoyl)-amino]-acetylamino}-acetic acid tert-butyl ester

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Technology Process of {2-cyclohexyl-2-[(2-hydroxy-ethyl)-(2-methanesulfonylamino-benzoyl)-amino]-acetylamino}-acetic acid tert-butyl ester

There total 2 articles about {2-cyclohexyl-2-[(2-hydroxy-ethyl)-(2-methanesulfonylamino-benzoyl)-amino]-acetylamino}-acetic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 934420-84-5
2-cyclohexyl-oxazolidine

: 162787-61-3
2-(methylsulfonamido)benzoic acid

: 2769-72-4
tert-Butyl isocyanoacetate

: 934421-09-7
{2-cyclohexyl-2-[(2-hydroxy-ethyl)-(2-methanesulfonylamino-benzoyl)-amino]-acetylamino}-acetic acid tert-butyl ester

Guidance literature:: With 3 A molecular sieve; In methanol; at 20 ℃; for 24h;
DOI:10.1021/jo062626z

Reference yield:

: 2043-61-0
cyclohexanecarbaldehyde

: 934421-09-7
{2-cyclohexyl-2-[(2-hydroxy-ethyl)-(2-methanesulfonylamino-benzoyl)-amino]-acetylamino}-acetic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: molecular sieves 4 Angstroem / diethyl ether / 1 h / 20 °C

2: 62 percent / molecular sieves 3 Angstroem / methanol / 24 h / 20 °C

With 3 A molecular sieve; 4 A molecular sieve; In methanol; diethyl ether; 2: Ugi reaction;
DOI:10.1021/jo062626z