dimethyl 5-propoxyisophthalate

Base Information

• Chemical Name: dimethyl 5-propoxyisophthalate
• CAS No.: 1055298-52-6
• Molecular Formula: C₁₃H₁₆O₅
• Molecular Weight: 252.267
• Mol file: 1055298-52-6.mol

Synonyms:dimethyl 5-propoxyisophthalate

Chemical Property of dimethyl 5-propoxyisophthalate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dimethyl 5-propoxyisophthalate

There total 3 articles about dimethyl 5-propoxyisophthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

Dimethyl 5-hydroxyisophthalate (13036-02-7) + propyl bromide (106-94-5) → dimethyl 5-propoxyisophthalate (1055298-52-6)

Guidance literature:

With potassium carbonate; In acetonitrile; for 42h; Heating;

DOI:10.1016/j.tet.2008.05.049

Reference yield:

5-Hydroxyisophthalic acid (618-83-7) → dimethyl 5-propoxyisophthalate (1055298-52-6)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfuric acid / Reflux

2: potassium carbonate / acetone / Reflux

With sulfuric acid; potassium carbonate; In acetone;

DOI:10.1039/c6dt00658b

Reference yield:

Dimethyl 5-hydroxyisophthalate (13036-02-7) → dimethyl 5-propoxyisophthalate (1055298-52-6)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1002/chem.201700848

upstream raw materials:

Dimethyl 5-hydroxyisophthalate

propyl bromide

5-Hydroxyisophthalic acid

Downstream raw materials:

(5-propoxy-1,3-phenylene)dimethanol