2-dodecyloxy-5-bromopropoxy-1,4-diiodobenzene

Base Information

• Chemical Name: 2-dodecyloxy-5-bromopropoxy-1,4-diiodobenzene
• CAS No.: 1140516-44-4
• Molecular Formula: C₂₁H₃₃BrI₂O₂
• Molecular Weight: 651.205

Synonyms:2-dodecyloxy-5-bromopropoxy-1,4-diiodobenzene

Chemical Property of 2-dodecyloxy-5-bromopropoxy-1,4-diiodobenzene

Chemical Property:

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Technology Process of 2-dodecyloxy-5-bromopropoxy-1,4-diiodobenzene

There total 1 articles about 2-dodecyloxy-5-bromopropoxy-1,4-diiodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

1-dodecyloxy-4-bromopropoxybenzene (1140516-42-2) → 2-dodecyloxy-5-bromopropoxy-1,4-diiodobenzene (1140516-44-4)

Guidance literature:

With mercury(II) diacetate; iodine; In dichloromethane; at 20 ℃; for 4h;

DOI:10.1021/ja809613n

Reference yield: 85.0%

2-dodecyloxy-5-bromopropoxy-1,4-diiodobenzene (1140516-44-4) + adenine (66224-66-6,66224-67-7,66224-68-8,66224-69-9,134434-48-3,134434-49-4,134454-76-5,134461-75-9) → C26H37I2N5O2 (1140516-46-6)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 60 ℃; Inert atmosphere;

DOI:10.1021/ja809613n

Reference yield: 67.0%

2-dodecyloxy-5-bromopropoxy-1,4-diiodobenzene (1140516-44-4) + thymin (65-71-4,28806-14-6,691841-57-3) → C26H38I2N2O4 (1140516-48-8)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; Inert atmosphere;

DOI:10.1021/ja809613n

upstream raw materials:

1-dodecyloxy-4-bromopropoxybenzene

Downstream raw materials:

C₂₆H₃₈I₂N₂O₄

C₂₆H₃₇I₂N₅O₂

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